HISHICOLIN PX-4MC

Base Information

• Chemical Name: HISHICOLIN PX-4MC
• CAS No.: 2304-24-7
• Molecular Formula: C13H30 P . Cl
• Molecular Weight: 252.808
• Mol file: 2304-24-7.mol

Synonyms:Phosphonium,tributylmethyl-, chloride (8CI,9CI); Tributylmethylphosphonium chloride (7CI);Methyltributylphosphonium chloride

Chemical Property of HISHICOLIN PX-4MC

Chemical Property:

• PSA: 13.59000
• LogP: 2.03810

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of HISHICOLIN PX-4MC

There total 6 articles about HISHICOLIN PX-4MC which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.5%

tri-n-butyl(methyl)phosphonium methyl carbonate (120256-45-3) → methyltributylphosphonium chloride (2304-24-7)

Guidance literature:

With hydrogenchloride; In methanol; water; at 20 ℃;

DOI:10.1039/c1dt10466g

Reference yield: 91.0%

tri(n-butyl)-methylenephosphorane (29218-85-7) + acetyl chloride (75-36-5) → methyltributylphosphonium chloride (2304-24-7) + (Acetylmethylen)tri(n-butyl)phosphoran (39743-80-1)

Guidance literature:

In diethyl ether; 1) -40 deg C, 2) 25 deg C, 2 h;

Reference yield:

methylmagnesium chloride (676-58-4) + tri-n-butylchlorophosphonium chloride → methyltributylphosphonium chloride (2304-24-7)

Guidance literature:

methylmagnesium chloride; tri-n-butylchlorophosphonium chloride; In tetrahydrofuran; dichloromethane; at 0 ℃; for 0.75h; Inert atmosphere;

With hydrogenchloride; In diethyl ether; water; for 0.166667h;

DOI:10.1039/c8cc02173b

upstream raw materials:

tri(n-butyl)-methylenephosphorane

acetyl chloride

tributylphosphine

Chloromethyltrimethylsilane

Downstream raw materials:

tri(n-butyl)-methylenephosphorane

tri-n-butyl(methyl)phosphonium dimethyl phosphate