BIS(3-AMINOPROPYL) ETHER

Base Information

• Chemical Name: BIS(3-AMINOPROPYL) ETHER
• CAS No.: 2157-24-6
• Molecular Formula: C6H16 N2 O
• Molecular Weight: 132.206
• Hs Code.: 2922199090
• Mol file: 2157-24-6.mol

Synonyms:Ether,bis(3-aminopropyl) (4CI); Propylamine, 3,3'-oxybis- (6CI,7CI,8CI);(7-Amino-4-oxaheptyl)amine; 1,7-Diamino-4-oxaheptane; 3,3'-Oxybis(propylamine);3-(3-Aminopropoxy)propylamine; Bis(3-aminopropyl) ether; Bis(g-aminopropyl) ether

Chemical Property of BIS(3-AMINOPROPYL) ETHER

Chemical Property:

• Vapor Pressure: 0.094mmHg at 25°C
• Refractive Index: 1.459
• Boiling Point: 72oC / 4mmHg
• PKA: 10.05±0.10(Predicted)
• Flash Point: 92.759oC
• PSA: 61.27000
• Density: 0.94 g/cm3
• LogP: 1.10120

Purity/Quality:

98%,99%, ^*data from raw suppliers

Bis(3-aminopropyl) Ether ^*data from reagent suppliers

Safty Information:

• Statements: 10-34
• Safety Statements: 16-24/25

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of BIS(3-AMINOPROPYL) ETHER

There total 1 articles about BIS(3-AMINOPROPYL) ETHER which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-cyanoethyl ether (1656-48-0) + ammonia (7664-41-7) → propylamine (107-10-8,42939-71-9) + bis(3-aminopropyl)ether (2157-24-6) + propan-1-ol-3-amine (156-87-6)

Guidance literature:

at 110 - 115 ℃; under 73550.8 Torr; Hydrogenation;

DOI:10.1021/ja01233a019 DOI:10.1021/ja01227a039

Reference yield: 97.0%

formaldehyd (50-00-0,30525-89-4,61233-19-0) + bis(3-aminopropyl)ether (2157-24-6) + diphenylphosphane (829-85-6) → C58H60N2OP4 (1264172-31-7)

Guidance literature:

formaldehyd; diphenylphosphane; In methanol; at 70 ℃; for 0.166667h; Inert atmosphere;

bis(3-aminopropyl)ether; In methanol; toluene; at 20 ℃; Inert atmosphere;

DOI:10.1002/adsc.200900377

Reference yield: 92.0%

bis(3-aminopropyl)ether (2157-24-6) + 2-Nitrobenzenesulfonyl chloride (1694-92-4) → N,N'-bis(2-nitrobenzenesulfonyl)-bis(3-aminopropyl) ether (344950-59-0)

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃; Inert atmosphere;

DOI:10.1021/jm901530b

upstream raw materials:

2-cyanoethyl ether

ammonia

Downstream raw materials:

bis-[3-(2,4-dinitro-anilino)-propyl]-ether

C₂₂H₂₂F₆N₂O₅

n-octyl carbamate