(3-tert-butoxycarbonyl-2-methoxy-phenyl)methylboronic acid (-)-pinanediolato diester

Base Information

Chemical Name:(3-tert-butoxycarbonyl-2-methoxy-phenyl)methylboronic acid (-)-pinanediolato diester
CAS No.:1613269-60-5
Molecular Formula:C₂₃H₃₃BO₅
Molecular Weight:400.323
Hs Code.:

Synonyms:(3-tert-butoxycarbonyl-2-methoxy-phenyl)methylboronic acid (-)-pinanediolato diester

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Chemical Property of (3-tert-butoxycarbonyl-2-methoxy-phenyl)methylboronic acid (-)-pinanediolato diester

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Technology Process of (3-tert-butoxycarbonyl-2-methoxy-phenyl)methylboronic acid (-)-pinanediolato diester

There total 5 articles about (3-tert-butoxycarbonyl-2-methoxy-phenyl)methylboronic acid (-)-pinanediolato diester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: chloro-methylboronic acid (-)-pinanediolato diester

: 1613269-59-2
3-iodo-2-methoxybenzoic acid tert-butyl ester

: 1613269-60-5
(3-tert-butoxycarbonyl-2-methoxy-phenyl)methylboronic acid (-)-pinanediolato diester

Guidance literature:: 3-iodo-2-methoxybenzoic acid tert-butyl ester; With TurboGrignard; In tetrahydrofuran; at -40 ℃; for 0.333333h;

chloro-methylboronic acid (-)-pinanediolato diester; In tetrahydrofuran; at -78 ℃; for 0.75h;

With zinc(II) chloride; In tetrahydrofuran; diethyl ether; for 2h;

Reference yield:

: 874347-49-6
3-iodo-2-methoxy-benzaldehyde

: 1613269-60-5
(3-tert-butoxycarbonyl-2-methoxy-phenyl)methylboronic acid (-)-pinanediolato diester

Guidance literature:: Multi-step reaction with 4 steps

1.1: 2,3-Dimethyl-2-butene; disodium hydrogen phosphate monohydrate; sodium chlorite / water; tert-butyl alcohol / 0.33 h

2.1: thionyl chloride / 0.5 h / 82 °C

3.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / -5 °C

3.2: 1.5 h

4.1: TurboGrignard / tetrahydrofuran / 0.33 h / -40 °C

4.2: 0.75 h / -78 °C

4.3: 2 h

With sodium chlorite; TurboGrignard; n-butyllithium; thionyl chloride; 2,3-Dimethyl-2-butene; disodium hydrogen phosphate monohydrate; In tetrahydrofuran; hexane; water; tert-butyl alcohol;

Reference yield:

: 879498-16-5
3-iodo-2-methoxy-benzoic acid

: 1613269-60-5
(3-tert-butoxycarbonyl-2-methoxy-phenyl)methylboronic acid (-)-pinanediolato diester

Guidance literature:: Multi-step reaction with 3 steps

1.1: thionyl chloride / 0.5 h / 82 °C

2.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / -5 °C

2.2: 1.5 h

3.1: TurboGrignard / tetrahydrofuran / 0.33 h / -40 °C

3.2: 0.75 h / -78 °C

3.3: 2 h

With TurboGrignard; n-butyllithium; thionyl chloride; In tetrahydrofuran; hexane;