Technology Process of N-(2-Cyanomethylphenyl)anthranilsaeuremethylester
There total 6 articles about N-(2-Cyanomethylphenyl)anthranilsaeuremethylester which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 68 percent / K2CO3 / Cu; CuI / dibutyl ether / 22 h / 175 °C
2: 99 percent / aq. HCl / acetone / 1.5 h / 30 °C
3: 99 percent / NaBH4 / diethyl ether / Heating
4: SOCl2; pyridine / diethyl ether / 1 h
5: dimethylsulfoxide / 1 h / 40 °C
With
pyridine; hydrogenchloride; sodium tetrahydroborate; thionyl chloride; potassium carbonate;
copper(l) iodide; copper;
In
diethyl ether; dibutyl ether; dimethyl sulfoxide; acetone;
1: Substitution / 2: Ring cleavage / 3: Reduction / 4: Chlorination / 5: Substitution;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 68 percent / K2CO3 / Cu; CuI / dibutyl ether / 22 h / 175 °C
2: 99 percent / aq. HCl / acetone / 1.5 h / 30 °C
3: 99 percent / NaBH4 / diethyl ether / Heating
4: SOCl2; pyridine / diethyl ether / 1 h
5: dimethylsulfoxide / 1 h / 40 °C
With
pyridine; hydrogenchloride; sodium tetrahydroborate; thionyl chloride; potassium carbonate;
copper(l) iodide; copper;
In
diethyl ether; dibutyl ether; dimethyl sulfoxide; acetone;
1: Substitution / 2: Ring cleavage / 3: Reduction / 4: Chlorination / 5: Substitution;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 99 percent / NaBH4 / diethyl ether / Heating
2: SOCl2; pyridine / diethyl ether / 1 h
3: dimethylsulfoxide / 1 h / 40 °C
With
pyridine; sodium tetrahydroborate; thionyl chloride;
In
diethyl ether; dimethyl sulfoxide;
1: Reduction / 2: Chlorination / 3: Substitution;