N1-(4-Methoxybenzyl)-N1-methylethane-1,2-diamine

Base Information

Chemical Name:N1-(4-Methoxybenzyl)-N1-methylethane-1,2-diamine
CAS No.:933737-03-2
Molecular Formula:C₁₁H₁₈N₂O
Molecular Weight:194.277
Hs Code.:
DSSTox Substance ID:DTXSID701199091
Mol file:933737-03-2.mol

Synonyms:933737-03-2;N*1*-(4-Methoxy-benzyl)-N*1*-methyl-ethane-1,2-diamine;N1-(4-Methoxybenzyl)-N1-methylethane-1,2-diamine;N'-[(4-methoxyphenyl)methyl]-N'-methylethane-1,2-diamine;(2-AMINOETHYL)[(4-METHOXYPHENYL)METHYL]METHYLAMINE;N'-[(4-methoxyphenyl)methyl]-N'-methyl-ethane-1,2-diamine;SCHEMBL17312007;DTXSID701199091;AM101643;EN300-1721681;N1-[(4-Methoxyphenyl)methyl]-N1-methyl-1,2-ethanediamine

Suppliers and Price of N1-(4-Methoxybenzyl)-N1-methylethane-1,2-diamine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
N1-(4-Methoxybenzyl)-N1-methylethane-1,2-diamine 97%
1g
$ 635.00

Total 1 raw suppliers

Chemical Property of N1-(4-Methoxybenzyl)-N1-methylethane-1,2-diamine

Chemical Property:

XLogP3:0.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:5
Exact Mass:194.141913202
Heavy Atom Count:14
Complexity:144

Purity/Quality:: N1-(4-Methoxybenzyl)-N1-methylethane-1,2-diamine 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CN(CCN)CC1=CC=C(C=C1)OC

Technology Process of N1-(4-Methoxybenzyl)-N1-methylethane-1,2-diamine

There total 3 articles about N1-(4-Methoxybenzyl)-N1-methylethane-1,2-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 127780-69-2
2-((4-methoxybenzyl)(methyl)amino)acetonitrile

: 933737-03-2
N₁-(4-methoxybenzyl)-N₁-methylethane-1,2-diamine

Guidance literature:: 2-((4-methoxybenzyl)(methyl)amino)acetonitrile; With lithium aluminium tetrahydride; In tetrahydrofuran; at -20 - 20 ℃; for 2h;

With water; Rochelle's salt; at -10 ℃;

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 933737-03-2
N₁-(4-methoxybenzyl)-N₁-methylethane-1,2-diamine

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium tetrahydroborate; water / methanol / 15 - 20 °C / Cooling with ice

2.1: N-ethyl-N,N-diisopropylamine / toluene / 1 h / Reflux

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / -20 - 20 °C

3.2: -10 °C

With sodium tetrahydroborate; lithium aluminium tetrahydride; water; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; toluene;

Reference yield:

: 702-24-9
4-methoxy-N-methylbenzylamine

: 933737-03-2
N₁-(4-methoxybenzyl)-N₁-methylethane-1,2-diamine

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-ethyl-N,N-diisopropylamine / toluene / 1 h / Reflux

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / -20 - 20 °C

2.2: -10 °C

With lithium aluminium tetrahydride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; toluene;