4-amino-N'-hydroxy-N-(2-{[4-methoxybenzyl](methyl)amino}ethyl)-1,2,5-oxadiazole-3-carboximidamide

Base Information

Chemical Name:4-amino-N'-hydroxy-N-(2-{[4-methoxybenzyl](methyl)amino}ethyl)-1,2,5-oxadiazole-3-carboximidamide
CAS No.:1608129-03-8
Molecular Formula:C₁₄H₂₀N₆O₃
Molecular Weight:320.351
Hs Code.:

Synonyms:4-amino-N'-hydroxy-N-(2-{[4-methoxybenzyl](methyl)amino}ethyl)-1,2,5-oxadiazole-3-carboximidamide

Suppliers and Price of 4-amino-N'-hydroxy-N-(2-{[4-methoxybenzyl](methyl)amino}ethyl)-1,2,5-oxadiazole-3-carboximidamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-amino-N'-hydroxy-N-(2-{[4-methoxybenzyl](methyl)amino}ethyl)-1,2,5-oxadiazole-3-carboximidamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-amino-N'-hydroxy-N-(2-{[4-methoxybenzyl](methyl)amino}ethyl)-1,2,5-oxadiazole-3-carboximidamide

There total 4 articles about 4-amino-N'-hydroxy-N-(2-{[4-methoxybenzyl](methyl)amino}ethyl)-1,2,5-oxadiazole-3-carboximidamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 933737-03-2
N₁-(4-methoxybenzyl)-N₁-methylethane-1,2-diamine

: 147085-13-0
4-amino-N-hydroxy-1,2,5-oxadiazole-3-carboximidamidoyl chloride

: 1608129-03-8
4-amino-N'-hydroxy-N-(2-{[4-methoxybenzyl](methyl)amino}ethyl)-1,2,5-oxadiazole-3-carboximidamide

Guidance literature:: With triethylamine; In tetrahydrofuran; ethyl acetate; at 25 ℃; for 1.5h;

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 1608129-03-8
4-amino-N'-hydroxy-N-(2-{[4-methoxybenzyl](methyl)amino}ethyl)-1,2,5-oxadiazole-3-carboximidamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium tetrahydroborate; water / methanol / 15 - 20 °C / Cooling with ice

2.1: N-ethyl-N,N-diisopropylamine / toluene / 1 h / Reflux

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / -20 - 20 °C

3.2: -10 °C

4.1: triethylamine / ethyl acetate; tetrahydrofuran / 1.5 h / 25 °C

With sodium tetrahydroborate; lithium aluminium tetrahydride; water; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; ethyl acetate; toluene;

Reference yield:

: 702-24-9
4-methoxy-N-methylbenzylamine

: 1608129-03-8
4-amino-N'-hydroxy-N-(2-{[4-methoxybenzyl](methyl)amino}ethyl)-1,2,5-oxadiazole-3-carboximidamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: N-ethyl-N,N-diisopropylamine / toluene / 1 h / Reflux

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / -20 - 20 °C

2.2: -10 °C

3.1: triethylamine / ethyl acetate; tetrahydrofuran / 1.5 h / 25 °C

With lithium aluminium tetrahydride; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; ethyl acetate; toluene;