(E)-(S)-2-methyl-propane-2-sulfinic acid 1-(4-methoxy-phenyl)-methylideneamide

Base Information

Chemical Name:(E)-(S)-2-methyl-propane-2-sulfinic acid 1-(4-methoxy-phenyl)-methylideneamide
CAS No.:683226-92-8
Molecular Formula:C₁₂H₁₇NO₂S
Molecular Weight:239.338
Hs Code.:

Synonyms:(E)-(S)-2-methyl-propane-2-sulfinic acid 1-(4-methoxy-phenyl)-methylideneamide

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Chemical Property of (E)-(S)-2-methyl-propane-2-sulfinic acid 1-(4-methoxy-phenyl)-methylideneamide

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Technology Process of (E)-(S)-2-methyl-propane-2-sulfinic acid 1-(4-methoxy-phenyl)-methylideneamide

There total 1 articles about (E)-(S)-2-methyl-propane-2-sulfinic acid 1-(4-methoxy-phenyl)-methylideneamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 123-11-5
4-methoxy-benzaldehyde

: 343338-28-3
(S)-2-methylpropane-2-sulfinamide

: 683226-92-8
(E)-(S)-2-methyl-propane-2-sulfinic acid 1-(4-methoxy-phenyl)-methylideneamide

Guidance literature:: With copper(II) sulfate; In dichloromethane; for 24h; Inert atmosphere;
DOI:10.1080/00397910802654898

Reference yield: 86.0%

: 1165952-92-0
cyclohexa-1,4-diene

: 683226-92-8
(E)-(S)-2-methyl-propane-2-sulfinic acid 1-(4-methoxy-phenyl)-methylideneamide

: 1023377-79-8
(S)-2-methyl-propane-2-sulfinic acid [(S)-(R)-cyclohexa-2,4-dienyl-(4-methoxyphenyl)-methyl]-amide

: 1023378-00-8
(S)-2-methyl-propane-2-sulfinic acid [(S)-cyclohexa-2,5-dienyl-(4-methoxy-phenyl)-methyl]-amide

Guidance literature:: cyclohexa-1,4-diene; With N,N,N,N,-tetramethylethylenediamine; (2-methylpropyl)lithium; In tetrahydrofuran; hexane; at -78 ℃; for 1.5h; Inert atmosphere;

With magnesium chloride; In tetrahydrofuran; for 3h; Inert atmosphere;

(E)-(S)-2-methyl-propane-2-sulfinic acid 1-(4-methoxy-phenyl)-methylideneamide; In tetrahydrofuran; at -78 ℃; for 0.5h; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/ol800478q

Reference yield: 84.0%

: 75-46-7
trifluoromethan

: 683226-92-8
(E)-(S)-2-methyl-propane-2-sulfinic acid 1-(4-methoxy-phenyl)-methylideneamide

: (S)-2-methyl-N-[(1R)-2,2,2-trifluoro-1-(4-methoxyphenyl)ethyl]propane-2-sulfinamide

Guidance literature:: trifluoromethan; (E)-(S)-2-methyl-propane-2-sulfinic acid 1-(4-methoxy-phenyl)-methylideneamide; In toluene; at -78 ℃; for 0.25h; Glovebox; Inert atmosphere;

With phosphazene base-P₄-tert-butyl; In hexane; at -78 ℃; Solvent; Temperature;