O-benzyl-N-methyl benzohydroxamic acid

Base Information

• Chemical Name: O-benzyl-N-methyl benzohydroxamic acid
• CAS No.: 22181-31-3
• Molecular Formula: C₁₅H₁₅NO₂
• Molecular Weight: 241.29

Synonyms:O-benzyl-N-methyl benzohydroxamic acid

Chemical Property of O-benzyl-N-methyl benzohydroxamic acid

Chemical Property:

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Technology Process of O-benzyl-N-methyl benzohydroxamic acid

There total 4 articles about O-benzyl-N-methyl benzohydroxamic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

methanol (67-56-1) + N-benzyloxy benzamide (3532-25-0) → O-benzyl-N-methyl benzohydroxamic acid (22181-31-3)

Guidance literature:

With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; at 25 ℃; for 20h;

DOI:10.1021/ja00543a021

Reference yield:

benzylphenylmethyl sulfonium fluoroborate (22900-27-2) + C6H5CONCH3O(1-)*Na(1+) → methyl-phenyl-thioether (100-68-5) + O-benzyl-N-methyl benzohydroxamic acid (22181-31-3)

Guidance literature:

In d⁽⁴⁾-methanol; at 30 ℃; Kinetics;

DOI:10.1021/jo981902+

Reference yield:

benzyl bromide (100-39-0) + C6H5CONCH3O(1-)*Na(1+) → O-benzyl-N-methyl benzohydroxamic acid (22181-31-3)

Guidance literature:

In isopropyl alcohol;

DOI:10.1021/jm00301a012

upstream raw materials:

benzyl bromide

methanol

N-benzyloxy benzamide

benzylphenylmethyl sulfonium fluoroborate

Downstream raw materials:

N-methyl-O-benzylhydroxylamine

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