(S,S)-2,3-bis(O-trimethylsilyl)-1,4-bisbutane-1,2,3,4-tetrol

Base Information

• Chemical Name: (S,S)-2,3-bis(O-trimethylsilyl)-1,4-bisbutane-1,2,3,4-tetrol
• CAS No.: 158835-58-6
• Molecular Formula: C₂₄H₃₈O₈S₂Si₂
• Molecular Weight: 574.864

Synonyms:(S,S)-2,3-bis(O-trimethylsilyl)-1,4-bisbutane-1,2,3,4-tetrol

Chemical Property of (S,S)-2,3-bis(O-trimethylsilyl)-1,4-bisbutane-1,2,3,4-tetrol

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Technology Process of (S,S)-2,3-bis(O-trimethylsilyl)-1,4-bisbutane-1,2,3,4-tetrol

There total 2 articles about (S,S)-2,3-bis(O-trimethylsilyl)-1,4-bisbutane-1,2,3,4-tetrol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

chloro-trimethyl-silane (75-77-4) + (2S,3S)-butane-1,4-diol bis[4-methylbenzenesulfonate] (57495-46-2,68138-99-8) + 1,1,1,3,3,3-hexamethyl-disilazane (999-97-3) → (S,S)-2,3-bis(O-trimethylsilyl)-1,4-bisbutane-1,2,3,4-tetrol (158835-58-6)

Guidance literature:

In dichloromethane; Ambient temperature;

DOI:10.1016/0957-4166(95)00257-P

Reference yield: 65.0%

(2S,3S)-butane-1,4-diol bis[4-methylbenzenesulfonate] (57495-46-2,68138-99-8) + 1,1,1,3,3,3-hexamethyl-disilazane (999-97-3) → (S,S)-2,3-bis(O-trimethylsilyl)-1,4-bisbutane-1,2,3,4-tetrol (158835-58-6)

Guidance literature:

With chloro-trimethyl-silane; In dichloromethane; for 12h; Ambient temperature;

DOI:10.1016/0040-4039(94)88078-6

Reference yield: 89.0%

Acetol acetate (592-20-1) + (S,S)-2,3-bis(O-trimethylsilyl)-1,4-bisbutane-1,2,3,4-tetrol (158835-58-6) → (S,S)-2-(acetoxymethyl)-2-methyl-4,5-bis(p-toluenesulfonyloxymethyl)-1,3-dioxolane (171561-22-1)

Guidance literature:

With trimethylsilyl trifluoromethanesulfonate; In chloroform; Ambient temperature;

DOI:10.1016/0957-4166(95)00257-P

upstream raw materials:

(2S,3S)-butane-1,4-diol bis[4-methylbenzenesulfonate]

1,1,1,3,3,3-hexamethyl-disilazane

chloro-trimethyl-silane

Downstream raw materials:

(S,S)-2-(acetoxymethyl)-2-phenyl-4,5-bis(p-toluenesulfonyloxymethyl)-1,3-dioxolane

(S,S)-2-methyl-2-phenyl-4,5-bis(p-toluenesulfonyloxymethyl)-1,3-dioxolane

(S,S)-2-(acetoxymethyl)-2-methyl-4,5-bis(p-toluenesulfonyloxymethyl)-1,3-dioxolane

(S,S)-2-(2'-acetoxyphenyl)-4,5-bis(p-toluenesulfonyloxymethyl)-1,3-dioxolane

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