benzoic p-methoxybenzoic anhydride

Base Information

• Chemical Name: benzoic p-methoxybenzoic anhydride
• CAS No.: 58618-94-3
• Molecular Formula: C₁₅H₁₂O₄
• Molecular Weight: 256.258
• Mol file: 58618-94-3.mol

Synonyms:benzoic p-methoxybenzoic anhydride

Chemical Property of benzoic p-methoxybenzoic anhydride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of benzoic p-methoxybenzoic anhydride

There total 9 articles about benzoic p-methoxybenzoic anhydride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

benzoyl chloride (98-88-4) + 4-methoxybenzoic acid (100-09-4) → benzoic p-methoxybenzoic anhydride (58618-94-3)

Guidance literature:

With triethylamine; In tetrahydrofuran; at 0 ℃; for 1h; Inert atmosphere;

DOI:10.1039/c8ob00178b

Reference yield: 95.2%

4-methoxy-benzoyl chloride (100-07-2) + benzoic acid (65-85-0,8013-63-6) → benzoic p-methoxybenzoic anhydride (58618-94-3)

Guidance literature:

With P₄-VP; In dichloromethane; for 1h; Ambient temperature;

DOI:10.1016/S0040-4039(00)85100-X

Reference yield: 64.0%

tetrakis-(4-methoxy-phenyl)-ethanone (19920-04-8) + dibenzoyl peroxide (94-36-0) → tris(4-methoxyphenyl)methanol (3010-81-9) + 1,1,2,2-tetrakis(4-methoxyphenyl)ethene (10019-24-6) + benzoic p-methoxybenzoic anhydride (58618-94-3) + 4-methoxybenzoic acid (100-09-4)

Guidance literature:

With boron trifluoride diethyl etherate; In 1,2-dichloro-ethane; at 50 ℃; for 24h; in a sealed tube;

upstream raw materials:

benzoyl-(4-methoxy-benzoyl)-peroxide

benzoyl chloride

4-methoxybenzoic acid

4-methoxy-benzoyl chloride

Downstream raw materials:

N-benzoylpiperidine

N-(p-methoxybenzoyl)piperidine

N-(p-methylphenyl)-p-methoxybenzamide

N-(4-methylphenyl)benzamide