3-Methoxy-2,8-dioxabicyclo[3.3.0]octane

Base Information

Chemical Name:3-Methoxy-2,8-dioxabicyclo[3.3.0]octane
CAS No.:213833-82-0
Molecular Formula:C₇H₁₂O₃
Molecular Weight:144.17
Hs Code.:
DSSTox Substance ID:DTXSID601292115
Nikkaji Number:J1.538.914A

Synonyms:DTXSID601292115;Hexahydro-2-methoxyfuro[2,3-b]furan;213833-82-0;3-Methoxy-2,8-dioxabicyclo[3.3.0]octane;(+/-)-2-methoxy-hexahydrofuro[2,3-b]furan

Suppliers and Price of 3-Methoxy-2,8-dioxabicyclo[3.3.0]octane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-Methoxy-2,8-dioxabicyclo[3.3.0]octane

Chemical Property:

XLogP3:0.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:1
Exact Mass:144.078644241
Heavy Atom Count:10
Complexity:126

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:COC1CC2CCOC2O1

Technology Process of 3-Methoxy-2,8-dioxabicyclo[3.3.0]octane

There total 1 articles about 3-Methoxy-2,8-dioxabicyclo[3.3.0]octane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 67-56-1
methanol

: 104223-37-2
hexahydro furo<2,3-b>furan-2-one

: 213833-82-0
(+/-)-2-methoxyhexahydrofuro[2,3-b]furan

: 26457-63-6
hexahydrofuro[2,3-b]furan

Guidance literature:: hexahydro furo<2,3-b>furan-2-one; With diisobutylaluminium hydride; In toluene; at -78 ℃; for 1.5h;

methanol; With boron trifluoride diethyl etherate; In toluene; at -78 - -60 ℃; for 0.0833333h;
DOI:10.1021/jo991151r

Reference yield: 40.0%

: 213833-70-6
(3R,5R)-(5-isopropenyl-2,3-dimethylcyclohex-1-enyloxy)trimethylsilane

: 213833-82-0
(+/-)-2-methoxyhexahydrofuro[2,3-b]furan

: 213833-77-3
(2R,3R,5R)-2-[(2R,3aS,6aR)-2,3,3a,4,5,6a-hexahydrofluoro[2,3-b]furan-2-yl]-5-isopropenyl-2,3-dimethylcyclohexanone

: 213833-81-9
(2R,3R,5R,2'R,3a'S,6a'R)-2-(hexahydrofuro[2,3-b]furan-2'-yl)-5-isopropenyl-2,3-dimethylcyclohexanone

Guidance literature:: With trityl perchlorate; In dichloromethane; at -78 ℃; for 78h;
DOI:10.1021/jo991151r

Reference yield: 35.0%

: 917-64-6
methyl magnesium iodide

: 6485-40-1,2244-16-8
(R)-Carvone

: 213833-82-0
(+/-)-2-methoxyhexahydrofuro[2,3-b]furan

: 213833-81-9
(2R,3R,5R,2'R,3a'S,6a'R)-2-(hexahydrofuro[2,3-b]furan-2'-yl)-5-isopropenyl-2,3-dimethylcyclohexanone

Guidance literature:: methyl magnesium iodide; (R)-Carvone; With chloro-trimethyl-silane; copper(I) bromide dimethylsulfide complex;

(+/-)-2-methoxyhexahydrofuro[2,3-b]furan; With triphenylmethylium hexachloroantimonate(V); In dichloromethane; at -78 ℃;
DOI:10.1016/S0040-4020(00)00110-1