4-[Ethylsulfanyl-(4-methoxy-phenyl)-methylene]-morpholin-4-ium; iodide

Base Information

• Chemical Name: 4-[Ethylsulfanyl-(4-methoxy-phenyl)-methylene]-morpholin-4-ium; iodide
• CAS No.: 120290-10-0
• Molecular Formula: C₁₄H₂₀NO₂S*I
• Molecular Weight: 393.289
• Mol file: 120290-10-0.mol

Synonyms:4-[Ethylsulfanyl-(4-methoxy-phenyl)-methylene]-morpholin-4-ium; iodide

Chemical Property of 4-[Ethylsulfanyl-(4-methoxy-phenyl)-methylene]-morpholin-4-ium; iodide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of 4-[Ethylsulfanyl-(4-methoxy-phenyl)-methylene]-morpholin-4-ium; iodide

There total 1 articles about 4-[Ethylsulfanyl-(4-methoxy-phenyl)-methylene]-morpholin-4-ium; iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-(4-methoxy-thiobenzoyl)-morpholine (6392-01-4) + ethyl iodide (75-03-6) → 4-[Ethylsulfanyl-(4-methoxy-phenyl)-methylene]-morpholin-4-ium; iodide (120290-10-0)

Guidance literature:

DOI:10.1016/S0040-4039(00)82188-7

Reference yield:

4-[Ethylsulfanyl-(4-methoxy-phenyl)-methylene]-morpholin-4-ium; iodide (120290-10-0) → 4-methoxy-benzaldehyde (123-11-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 91 percent Spectr_. / trimethoxysilane, (LiOCHMe)2 / tetrahydrofuran / 3 h / 0 °C

2: H₂O / TCL

With trimethoxysilane; (LiOCHMe)2; water; In tetrahydrofuran;

DOI:10.1016/S0040-4039(00)82188-7

Reference yield:

4-[Ethylsulfanyl-(4-methoxy-phenyl)-methylene]-morpholin-4-ium; iodide (120290-10-0) → 4-[ethylsulfanyl-(4-methoxy-phenyl)-methyl]-morpholine (70227-33-7)

Guidance literature:

With trimethoxysilane; (LiOCHMe)2; In tetrahydrofuran; at 0 ℃; for 3h;

DOI:10.1016/S0040-4039(00)82188-7

upstream raw materials:

N-(4-methoxy-thiobenzoyl)-morpholine

ethyl iodide

Downstream raw materials:

4-[ethylsulfanyl-(4-methoxy-phenyl)-methyl]-morpholine

4-methoxy-benzaldehyde