C₁₆H₁₈FN₃O

Base Information

Chemical Name:C₁₆H₁₈FN₃O
CAS No.:1398048-25-3
Molecular Formula:C₁₆H₁₈FN₃O
Molecular Weight:287.337
Hs Code.:

C<sub>16</sub>H<sub>18</sub>FN<sub>3</sub>O

Synonyms:C₁₆H₁₈FN₃O

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₆H₁₈FN₃O

Chemical Property:

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Technology Process of C₁₆H₁₈FN₃O

There total 4 articles about C₁₆H₁₈FN₃O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 7677-24-9
trimethylsilyl cyanide

: 1398048-23-1
C₁₂H₁₃FN₂O

: 67-64-1
acetone

: 1398048-25-3
C₁₆H₁₈FN₃O

Guidance literature:: With zinc(II) chloride; In 1,4-dioxane; at 20 ℃; for 3h;

Reference yield:

: 188975-47-5
dimethyl 2-(2-fluoro-4-nitrophenyl)malonate

: 1398048-25-3
C₁₆H₁₈FN₃O

Guidance literature:: Multi-step reaction with 6 steps

1: sodium methylate / methanol / 20 °C / Inert atmosphere

2: water; sodium chloride / dimethyl sulfoxide / 24 h / 155 °C / Inert atmosphere

3: ammonium hydroxide; methanol / 48 h / 20 °C

4: polyphosphoric acid / 3 h / 160 °C

5: ammonium chloride; iron / water; methanol / 2 h / 90 °C / Inert atmosphere

6: zinc(II) chloride / 1,4-dioxane / 3 h / 20 °C

With methanol; ammonium hydroxide; water; sodium methylate; iron; ammonium chloride; sodium chloride; zinc(II) chloride; In 1,4-dioxane; methanol; water; dimethyl sulfoxide;

Reference yield:

: 1146975-15-6
Trimethyl 1-(2-fluoro-4-nitrophenyl)propane-1,1,3-tricarboxylate

: 1398048-25-3
C₁₆H₁₈FN₃O

Guidance literature:: Multi-step reaction with 5 steps

1: water; sodium chloride / dimethyl sulfoxide / 24 h / 155 °C / Inert atmosphere

2: ammonium hydroxide; methanol / 48 h / 20 °C

3: polyphosphoric acid / 3 h / 160 °C

4: ammonium chloride; iron / water; methanol / 2 h / 90 °C / Inert atmosphere

5: zinc(II) chloride / 1,4-dioxane / 3 h / 20 °C

With methanol; ammonium hydroxide; water; iron; ammonium chloride; sodium chloride; zinc(II) chloride; In 1,4-dioxane; methanol; water; dimethyl sulfoxide;