1,2-bis(trimethylsilyl)-1,1,2,2-tetrafluoroethane

Base Information

Chemical Name:1,2-bis(trimethylsilyl)-1,1,2,2-tetrafluoroethane
CAS No.:186824-44-2
Molecular Formula:C₈H₁₈F₄Si₂
Molecular Weight:246.396
Hs Code.:

Synonyms:1,2-bis(trimethylsilyl)-1,1,2,2-tetrafluoroethane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2-bis(trimethylsilyl)-1,1,2,2-tetrafluoroethane

Chemical Property:

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Technology Process of 1,2-bis(trimethylsilyl)-1,1,2,2-tetrafluoroethane

There total 3 articles about 1,2-bis(trimethylsilyl)-1,1,2,2-tetrafluoroethane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 115262-00-5
[chloro(difluoro)methyl]trimethylsilane

: 107-46-0
Hexamethyldisiloxane

: 86847-53-2
bis(trimethylsilyl)difluoromethane

: 186824-44-2
1,2-bis(trimethylsilyl)-1,1,2,2-tetrafluoroethane

Guidance literature:: With chloro-trimethyl-silane; Tris(3,6-dioxaheptyl)amine; tetrabutylammomium bromide; In tetrahydrofuran; Yields of byproduct given; electrolysis, Al anode, Ni cathode, other reagents: hexamethylphosphoramide, tetrabutylammonium hexafluorophosphate;
DOI:10.1021/ja962990n

Reference yield:

: 75-77-4
chloro-trimethyl-silane

: 75-61-6
dibromodifluoromethane

: 420-56-4
trimethylsilyl fluoride

: 86847-53-2
bis(trimethylsilyl)difluoromethane

: 186824-44-2
1,2-bis(trimethylsilyl)-1,1,2,2-tetrafluoroethane

Guidance literature:: Yield given. Yields of byproduct given. Title compound not separated from byproducts; electrolysis;
DOI:10.1021/ja962990n

Reference yield:

: 75-77-4
chloro-trimethyl-silane

: 115262-00-5
[chloro(difluoro)methyl]trimethylsilane

: 420-56-4
trimethylsilyl fluoride

: 65864-64-4
trimethyl(difluoromethyl)silane

: 86847-53-2
bis(trimethylsilyl)difluoromethane

: 186824-44-2
1,2-bis(trimethylsilyl)-1,1,2,2-tetrafluoroethane

Guidance literature:: With N,N,N,N,N,N-hexamethylphosphoric triamide; tetrabutylammomium bromide; In tetrahydrofuran; Mechanism; Product distribution; electrolysis, Al anode, Ni cathode, other reagents: tris(3,6-dioxaheptyl)amine, tetrabutylammonium hexafluorophosphate, magnesium, various current density, various reactant ratios;
DOI:10.1021/ja962990n