N,N-DIMETHYL-3,5-DINITROANILINE

Base Information

• Chemical Name: N,N-DIMETHYL-3,5-DINITROANILINE
• CAS No.: 46429-76-9
• Molecular Formula: C8H9 N3 O4
• Molecular Weight: 211.17
• Hs Code.: 2921430090
• Mol file: 46429-76-9.mol

Synonyms:N,N-Dimethyl-3,5-dinitroaniline

Chemical Property of N,N-DIMETHYL-3,5-DINITROANILINE

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Refractive Index: 1.628
• Boiling Point: 342.848°C at 760 mmHg
• Flash Point: 161.149°C
• PSA: 94.88000
• Density: 1.397g/cm³
• LogP: 2.61540

Purity/Quality:

98%,99%, ^*data from raw suppliers

N,N-Dimethyl-3,5-dinitroaniline ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N,N-DIMETHYL-3,5-DINITROANILINE

There total 4 articles about N,N-DIMETHYL-3,5-DINITROANILINE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.3%

1,3,5-trinitrobenzene (99-35-4) + dimethyl amine (124-40-3) → N,N-dimethyl-3,5-dinitroaniline (46429-76-9)

Guidance literature:

In water; at 180 ℃; for 4h; chemoselective reaction; Autoclave;

DOI:10.3184/030823408X293198

Reference yield: 43.0%

N,N,N,N,N,N-hexamethylphosphoric triamide (680-31-9) + 1,3,5-trinitrobenzene (99-35-4) → N,N-dimethyl-3,5-dinitroaniline (46429-76-9)

Guidance literature:

at 155 - 160 ℃; for 10.5h;

DOI:10.1016/j.mencom.2013.05.019

Reference yield:

methanol (67-56-1) → N,N-dimethyl-3,5-dinitroaniline (46429-76-9)

Guidance literature:

DOI:10.1039/jr9490002785

upstream raw materials:

methanol

3, 5-dinitroaniline

1,3,5-trinitrobenzene

dimethyl amine

Refernces

• 1、 Chao, Qian,Jinqiang, Liu,Xinzhi, Chen. "Preparation of N-alkyl-substituted 3,5-dinitroanilines by amination of 1,3,5-trinitrobenzene". experimental part. p. 70 - 71. Retrieved 2009/07/18.