2,2-dimethylthiopropionic acid S-[(chloro)(phenoxy)phosphoryloxy]ethyl ester

Base Information

Chemical Name:2,2-dimethylthiopropionic acid S-[(chloro)(phenoxy)phosphoryloxy]ethyl ester
CAS No.:952513-67-6
Molecular Formula:C₁₃H₁₈ClO₄PS
Molecular Weight:336.776
Hs Code.:

Synonyms:2,2-dimethylthiopropionic acid S-[(chloro)(phenoxy)phosphoryloxy]ethyl ester

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Chemical Property of 2,2-dimethylthiopropionic acid S-[(chloro)(phenoxy)phosphoryloxy]ethyl ester

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Technology Process of 2,2-dimethylthiopropionic acid S-[(chloro)(phenoxy)phosphoryloxy]ethyl ester

There total 2 articles about 2,2-dimethylthiopropionic acid S-[(chloro)(phenoxy)phosphoryloxy]ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 770-12-7
O-phenyl phosphorodichloridate

: 153121-88-1
S-(2-hydroxyethyl) 2,2-dimethylpropanethioate

: 952513-67-6
2,2-dimethylthiopropionic acid S-[(chloro)(phenoxy)phosphoryloxy]ethyl ester

Guidance literature:: With triethylamine; In tetrahydrofuran;
DOI:10.1016/S0960-894X(98)00535-6

Reference yield:

: 3282-30-2
pivaloyl chloride

: 952513-67-6
2,2-dimethylthiopropionic acid S-[(chloro)(phenoxy)phosphoryloxy]ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 2 h / -78 - 20 °C

2: triethylamine / dichloromethane / 2 h / Inert atmosphere; Cooling with ice

With triethylamine; In dichloromethane;