o-(Methylthio)-phenyl ethyl sulphide

Base Information

Chemical Name:o-(Methylthio)-phenyl ethyl sulphide
CAS No.:83500-73-6
Molecular Formula:C₉H₁₂S₂
Molecular Weight:184.326
Hs Code.:

Synonyms:o-(Methylthio)-phenyl ethyl sulphide

Suppliers and Price of o-(Methylthio)-phenyl ethyl sulphide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of o-(Methylthio)-phenyl ethyl sulphide

Chemical Property:

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Technology Process of o-(Methylthio)-phenyl ethyl sulphide

There total 2 articles about o-(Methylthio)-phenyl ethyl sulphide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2388-68-3
o-bis(mercaptomethyl)benzene

: 74-88-4
methyl iodide

: 83500-73-6
o-(Methylthio)-phenyl ethyl sulphide

Guidance literature:: o-bis(mercaptomethyl)benzene; With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In diethyl ether; hexane; at 15 - 20 ℃; for 2h;

methyl iodide; In diethyl ether; hexane; at 0 - 20 ℃;
DOI:10.1016/S0040-4020(99)00873-X

Reference yield:

: 83500-76-9
o-(Isopropylthio)-phenyl methyl sulphide

: 75-03-6
ethyl iodide

: 83500-73-6
o-(Methylthio)-phenyl ethyl sulphide

Guidance literature:: With sodium methylate; Yield given. Multistep reaction; 1.) HMPT, 120 deg C, 15 h;
DOI:10.1055/s-1982-29844

Reference yield: 63.0%

: 75-77-4
chloro-trimethyl-silane

: 83500-73-6
o-(Methylthio)-phenyl ethyl sulphide

: ({[2-(ethylthio)phenyl]thio}methyl)(trimethyl)silane

Guidance literature:: o-(Methylthio)-phenyl ethyl sulphide; With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; In diethyl ether; hexane; at 15 - 20 ℃; for 2h;

chloro-trimethyl-silane; In diethyl ether; hexane; at 0 - 20 ℃;
DOI:10.1016/S0040-4020(99)00873-X