ethyl 3-((3-ethoxy-3-oxopropyl)(methyl)amino)-2-(4-fluorophenyl)propanoate

Base Information

Chemical Name:ethyl 3-((3-ethoxy-3-oxopropyl)(methyl)amino)-2-(4-fluorophenyl)propanoate
CAS No.:1310535-78-4
Molecular Formula:C₁₇H₂₄FNO₄
Molecular Weight:325.38
Hs Code.:

Synonyms:ethyl 3-((3-ethoxy-3-oxopropyl)(methyl)amino)-2-(4-fluorophenyl)propanoate

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Chemical Property of ethyl 3-((3-ethoxy-3-oxopropyl)(methyl)amino)-2-(4-fluorophenyl)propanoate

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Technology Process of ethyl 3-((3-ethoxy-3-oxopropyl)(methyl)amino)-2-(4-fluorophenyl)propanoate

There total 3 articles about ethyl 3-((3-ethoxy-3-oxopropyl)(methyl)amino)-2-(4-fluorophenyl)propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 1263870-41-2
ethyl 3-((3-ethoxy-3-oxopropyl)amino)-2-(4-fluorophenyl)propanoate

: 74-88-4
methyl iodide

: 1310535-78-4
ethyl 3-((3-ethoxy-3-oxopropyl)(methyl)amino)-2-(4-fluorophenyl)propanoate

Guidance literature:: With potassium carbonate; In acetone; at 20 ℃; for 2h;

Reference yield:

: 7054-58-2,15032-42-5
ethyl 2-cyano-2-(4-fluorophenyl)acetate

: 1310535-78-4
ethyl 3-((3-ethoxy-3-oxopropyl)(methyl)amino)-2-(4-fluorophenyl)propanoate

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen; sulfuric acid / palladium 10% on activated carbon / acetic acid / 18 h / 20 °C

2: ethanol / 18 h / 20 °C

3: potassium carbonate / acetone / 2 h / 0 - 20 °C

With sulfuric acid; hydrogen; potassium carbonate; palladium 10% on activated carbon; In ethanol; acetic acid; acetone;

Reference yield:

: 459-22-3
4-fluorophenylacetonitrile

: 1310535-78-4
ethyl 3-((3-ethoxy-3-oxopropyl)(methyl)amino)-2-(4-fluorophenyl)propanoate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / tetrahydrofuran / 0.25 h / -10 °C

1.2: 40 °C

2.1: hydrogen; sulfuric acid / palladium 10% on activated carbon / acetic acid / 18 h / 20 °C

3.1: ethanol / 18 h / 20 °C

4.1: potassium carbonate / acetone / 2 h / 0 - 20 °C

With sulfuric acid; hydrogen; sodium hydride; potassium carbonate; palladium 10% on activated carbon; In tetrahydrofuran; ethanol; acetic acid; acetone;