N-[4-(4-benzyloxy-2,6-dimethoxyphenyl)-5-methyl-2H-pyrazol-3-yl]acetamidine acetic acid salt

Base Information

Chemical Name:N-[4-(4-benzyloxy-2,6-dimethoxyphenyl)-5-methyl-2H-pyrazol-3-yl]acetamidine acetic acid salt
CAS No.:1217490-59-9
Molecular Formula:C₂H₄O₂*C₂₁H₂₄N₄O₃
Molecular Weight:440.499
Hs Code.:

Synonyms:N-[4-(4-benzyloxy-2,6-dimethoxyphenyl)-5-methyl-2H-pyrazol-3-yl]acetamidine acetic acid salt

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Chemical Property of N-[4-(4-benzyloxy-2,6-dimethoxyphenyl)-5-methyl-2H-pyrazol-3-yl]acetamidine acetic acid salt

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Technology Process of N-[4-(4-benzyloxy-2,6-dimethoxyphenyl)-5-methyl-2H-pyrazol-3-yl]acetamidine acetic acid salt

There total 5 articles about N-[4-(4-benzyloxy-2,6-dimethoxyphenyl)-5-methyl-2H-pyrazol-3-yl]acetamidine acetic acid salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 1217490-56-6
4-(4-benzyloxy-2,6-dimethoxyphenyl)-5-methyl-2H-pyrazol-3-ylamine

: 2208-07-3
ethyl acetimidate hydrochloride

: 64-19-7,77671-22-8
acetic acid

: 1217490-59-9
N-[4-(4-benzyloxy-2,6-dimethoxyphenyl)-5-methyl-2H-pyrazol-3-yl]acetamidine acetic acid salt

Guidance literature:: In acetonitrile; at 20 ℃; for 18h;
DOI:10.1002/jlcr.1616

Reference yield:

: 22080-96-2
syringaldehyde

: 1217490-59-9
N-[4-(4-benzyloxy-2,6-dimethoxyphenyl)-5-methyl-2H-pyrazol-3-yl]acetamidine acetic acid salt

Guidance literature:: Multi-step reaction with 5 steps

1: potassium carbonate / acetone / 14 h / Reflux

2: potassium tert-butylate / 1,2-dimethoxyethane / 3 h / -60 - -50 °C

3: sodium / 1.83 h / Reflux

4: hydrazine hydrate; acetic acid / toluene / 5 h / Reflux

5: acetonitrile / 18 h / 20 °C

With potassium tert-butylate; sodium; potassium carbonate; hydrazine hydrate; acetic acid; In 1,2-dimethoxyethane; acetone; toluene; acetonitrile;
DOI:10.1002/jlcr.1616

Reference yield:

: 1217490-53-3
(4-benzyloxy-2,6-dimethoxyphenyl)acetonitrile

: 1217490-59-9
N-[4-(4-benzyloxy-2,6-dimethoxyphenyl)-5-methyl-2H-pyrazol-3-yl]acetamidine acetic acid salt

Guidance literature:: Multi-step reaction with 3 steps

1: sodium / 1.83 h / Reflux

2: hydrazine hydrate; acetic acid / toluene / 5 h / Reflux

3: acetonitrile / 18 h / 20 °C

With sodium; hydrazine hydrate; acetic acid; In toluene; acetonitrile;
DOI:10.1002/jlcr.1616