N₁-(4-(3-bromopropoxy)phenyl)-N₁,N₄,N₄-tris(4-methoxyphenyl)benzene-1,4-diamine

Base Information

Chemical Name:N₁-(4-(3-bromopropoxy)phenyl)-N₁,N₄,N₄-tris(4-methoxyphenyl)benzene-1,4-diamine
CAS No.:1206195-89-2
Molecular Formula:C₃₆H₃₅BrN₂O₄
Molecular Weight:639.589
Hs Code.:

N<sub>1</sub>-(4-(3-bromopropoxy)phenyl)-N<sub>1</sub>,N<sub>4</sub>,N<sub>4</sub>-tris(4-methoxyphenyl)benzene-1,4-diamine

Synonyms:N₁-(4-(3-bromopropoxy)phenyl)-N₁,N₄,N₄-tris(4-methoxyphenyl)benzene-1,4-diamine

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Chemical Property of N₁-(4-(3-bromopropoxy)phenyl)-N₁,N₄,N₄-tris(4-methoxyphenyl)benzene-1,4-diamine

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Technology Process of N₁-(4-(3-bromopropoxy)phenyl)-N₁,N₄,N₄-tris(4-methoxyphenyl)benzene-1,4-diamine

There total 11 articles about N₁-(4-(3-bromopropoxy)phenyl)-N₁,N₄,N₄-tris(4-methoxyphenyl)benzene-1,4-diamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.2%

: 1206195-88-1
3-(4-((4-(bis(4-methoxyphenyl)amino)phenyl)(4-methoxyphenyl)amino)phenoxy)propyl methanesulfonate

: 1206195-89-2
N₁-(4-(3-bromopropoxy)phenyl)-N₁,N₄,N₄-tris(4-methoxyphenyl)benzene-1,4-diamine

Guidance literature:: With lithium bromide; In tetrahydrofuran; at 60 ℃; Inert atmosphere;

Reference yield:

: 194416-45-0
4-bromo-N,N-bis-(4-methoxyphenyl)aniline

: 1206195-89-2
N₁-(4-(3-bromopropoxy)phenyl)-N₁,N₄,N₄-tris(4-methoxyphenyl)benzene-1,4-diamine

Guidance literature:: Multi-step reaction with 4 steps

1.1: tri-tert-butyl phosphine; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; sodium t-butanolate / toluene / 90 °C / Inert atmosphere

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C / Inert atmosphere

3.1: dmap / tetrahydrofuran / 0.17 h / Cooling with ice; Inert atmosphere

3.2: 0.17 h

3.3: 0.08 h

4.1: lithium bromide / tetrahydrofuran / 60 °C / Inert atmosphere

With dmap; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tri-tert-butyl phosphine; tetrabutyl ammonium fluoride; lithium bromide; sodium t-butanolate; In tetrahydrofuran; toluene;

Reference yield:

: 1206195-86-9
N₁-(4-(3-(tert-butyldimethylsilyloxy)propoxy)phenyl)-N₁,N₄,N₄-tris(4-methoxyphenyl)benzene-1,4-diamine

: 1206195-89-2
N₁-(4-(3-bromopropoxy)phenyl)-N₁,N₄,N₄-tris(4-methoxyphenyl)benzene-1,4-diamine

Guidance literature:: Multi-step reaction with 3 steps

1: tetrabutyl ammonium fluoride / water; tetrahydrofuran

2: dmap; triethylamine / water; tetrahydrofuran

3: lithium bromide / water; tetrahydrofuran

With dmap; lithium bromide; tetrabutyl ammonium fluoride; triethylamine; In tetrahydrofuran; water;