Benzenepropanoic acid, 3-fluoro-, Methyl ester

Base Information

• Chemical Name: Benzenepropanoic acid, 3-fluoro-, Methyl ester
• CAS No.: 425704-52-5
• Molecular Formula: C₁₀H₁₁FO₂
• Molecular Weight: 182.195
• Hs Code.: 2916399090
• Mol file: 425704-52-5.mol

Synonyms:methyl 3-(3-fluorophenyl)propanoate

Chemical Property of Benzenepropanoic acid, 3-fluoro-, Methyl ester

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Methyl3-(3-fluorophenyl)propanoate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzenepropanoic acid, 3-fluoro-, Methyl ester

There total 10 articles about Benzenepropanoic acid, 3-fluoro-, Methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

methanol (67-56-1) + 3-(3-fluorophenyl)propionic acid (458-45-7) → methyl 3-(3-fluorophenyl)propanoate (425704-52-5)

Guidance literature:

With sulfuric acid; for 6h; Reflux;

Reference yield: 73.0%

methanol (67-56-1) + carbon monoxide (201230-82-2) + C31H25FN(1+)*BF4(1-) → methyl 3-(3-fluorophenyl)propanoate (425704-52-5)

Guidance literature:

With potassium hydrogencarbonate; cobalt(II) aceylacetonate; 1,10-phenanthroline-4,7-diol; In N,N-dimethyl-formamide; at 100 ℃; for 12h; under 15001.5 Torr; Autoclave;

DOI:10.1021/acs.orglett.9b02534

Reference yield:

methyl (E)-m-fluorocinnamate (74325-03-4) → methyl 3-(3-fluorophenyl)propanoate (425704-52-5)

Guidance literature:

With hydrogen; palladium on activated charcoal; In tetrahydrofuran; under 2068.59 Torr;

DOI:10.1021/jm010556c

upstream raw materials:

3-(3-fluorophenyl)propionic acid

diazomethyl-trimethyl-silane

methyl (E)-m-fluorocinnamate

3-Fluorobenzaldehyde

Downstream raw materials:

[4-(3-fluoro-phenyl)-2-oxo-butyl]-phosphonic acid dimethyl ester

3-(3-fluorophenyl)propan-1-ol

5-fluoro-1-indanone

3-(3-fluorophenyl)propanal

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