D-GLUCOSE PHENYLHYDRAZONE

Base Information

• Chemical Name: D-GLUCOSE PHENYLHYDRAZONE
• CAS No.: 3713-25-5
• Molecular Formula: C12H18 N2 O5
• Molecular Weight: 270.285
• Hs Code.: 2928000090
• Mol file: 3713-25-5.mol

Synonyms:D-Glucose,phenylhydrazone (6CI,7CI,8CI,9CI); Glucose phenylhydrazone

Chemical Property of D-GLUCOSE PHENYLHYDRAZONE

Chemical Property:

• Vapor Pressure: 2.96E-16mmHg at 25°C
• Refractive Index: 1.595
• Boiling Point: 620.5°Cat760mmHg
• Flash Point: 329°C
• PSA: 125.54000
• Density: 1.39g/cm³
• LogP: -1.40680

Purity/Quality:

98%Min ^*data from raw suppliers

D-GLUCOSE PHENYLHYDRAZONE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of D-GLUCOSE PHENYLHYDRAZONE

There total 10 articles about D-GLUCOSE PHENYLHYDRAZONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

D-glucose (50-99-7) + phenylhydrazine (100-63-0) → D-glucose phenylhydrazone (3713-25-5)

Guidance literature:

In water; at 20 ℃; for 4h;

DOI:10.1016/j.tetlet.2004.11.084

Reference yield:

β-D-glucose (492-61-5) + phenylhydrazine hydrochloride (59-88-1) → N-β-D-[glucopyranosyl]-N'-phenylhydrazine (10403-18-6) + α-D-glucopyranosylphenylhydrazine (35521-26-7) + D-glucose phenylhydrazone (3713-25-5)

Guidance literature:

With sodium acetate; In water; Overall yield = 29 %;

DOI:10.1002/ejoc.201600462

Reference yield:

→ D-glucose phenylhydrazone (3713-25-5)

Guidance literature:

With ethanol;

upstream raw materials:

ethanol

D-glucose

phenylhydrazine

water

Downstream raw materials:

3-(D-gluco-1,2,3,4,5-Pentahydroxy-pentyl)-1,5-diphenyl-formazan

1-Amino-1-deoxy-D-glucitol

1,5-diphenyl-3-benzeneazoformazane

galactose