Technology Process of 4'-nitro-2-phenoxy-1,1'-biphenyl
There total 7 articles about 4'-nitro-2-phenoxy-1,1'-biphenyl which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
palladium; potassium hydroxide;
In
water;
at 100 ℃;
for 1h;
Sealed tube;
Green chemistry;
DOI:10.1016/j.molcata.2013.07.012
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / -30 - 23 °C / Inert atmosphere; Schlenk technique
1.2: 2 h / Inert atmosphere; Schlenk technique; Reflux
1.3: 0.5 h / 23 °C / Inert atmosphere; Schlenk technique
2.1: tris-(dibenzylideneacetone)dipalladium(0); caesium carbonate / toluene; water / 17 h / 20 - 100 °C / Inert atmosphere; Schlenk technique
With
tris-(dibenzylideneacetone)dipalladium(0); n-butyllithium; caesium carbonate;
In
tetrahydrofuran; hexane; water; toluene;
2.1: |Suzuki-Miyaura Coupling;
DOI:10.1039/c3ob42065e
- Guidance literature:
-
Multi-step reaction with 3 steps
1: acetonitrile / 20 °C / Inert atmosphere
2: manganese(IV) oxide / dichloromethane / 20 °C / Inert atmosphere
3: manganese(IV) oxide / 160 °C
With
manganese(IV) oxide;
In
dichloromethane; acetonitrile;
DOI:10.1021/jo202406k
