6-methylthio-7-phenoxy-2',3'-dimethoxybenzooctem

Base Information

• Chemical Name: 6-methylthio-7-phenoxy-2',3'-dimethoxybenzo
• Molecular Formula: C₂₀H₂₁NO₄S
• Molecular Weight: 371.457

Synonyms:6-methylthio-7-phenoxy-2',3'-dimethoxybenzooctem

Chemical Property of 6-methylthio-7-phenoxy-2',3'-dimethoxybenzo

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

There total 5 articles about 6-methylthio-7-phenoxy-2',3'-dimethoxybenzooctem which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

6,7-dimethoxy-1-(methylsulfanyl)-3,4-dihydroisoquinoline (24456-60-8) + Phenoxyacetyl chloride (701-99-5) → 6-methylthio-7-phenoxy-2',3'-dimethoxybenzooctem (77670-15-6)

Guidance literature:

With triethylamine; In dichloromethane; Ambient temperature; 1 h (adding), then several hours;

DOI:10.1016/0040-4020(80)80195-5

Reference yield:

6,7-dimethoxy-3,4-dihydro-2H-isoquinolin-1-one (493-49-2) → 6-methylthio-7-phenoxy-2',3'-dimethoxybenzooctem (77670-15-6)

Guidance literature:

Multi-step reaction with 3 steps

1: 54 percent / phosphoruspentasulphide / pyridine / 2.5 h / Heating

2: 60 percent / CH₂Cl₂ / 2 h / Heating

3: 65 percent / triethylamine / CH₂Cl₂ / Ambient temperature; 1 h (adding), then several hours

With phosphorous (V) sulfide; triethylamine; In pyridine; dichloromethane;

DOI:10.1016/0040-4020(80)80195-5

Reference yield:

6,7-dimethoxy-3,4-dihydroisoquinoline-1(2H)-thione (24456-59-5) → 6-methylthio-7-phenoxy-2',3'-dimethoxybenzooctem (77670-15-6)

Guidance literature:

Multi-step reaction with 2 steps

1: 60 percent / CH₂Cl₂ / 2 h / Heating

2: 65 percent / triethylamine / CH₂Cl₂ / Ambient temperature; 1 h (adding), then several hours

With triethylamine; In dichloromethane;

DOI:10.1016/0040-4020(80)80195-5

upstream raw materials:

6,7-dimethoxy-1-(methylsulfanyl)-3,4-dihydroisoquinoline

Phenoxyacetyl chloride

2-phenoxyacetic acid

6,7-dimethoxy-3,4-dihydro-2H-isoquinolin-1-one

Downstream raw materials:

7-β-phenoxy-2',3'-dimethoxybenzooctem

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