Technology Process of C25H26N4O6
There total 7 articles about C25H26N4O6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
triethylamine;
1,1'-bis(diphenylphosphino)ferrocene; palladium diacetate;
In
methanol; dimethyl sulfoxide;
at 85 ℃;
under 760.051 Torr;
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: sodium carbonate / acetone / 24 h / Reflux
1.2: 1 h / 90 °C
2.1: potassium carbonate / toluene / 40 h / Reflux
3.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 1 h / 20 °C / Inert atmosphere
3.2: 2 h / 20 - 90 °C
4.1: ammonium acetate / 2.5 h / 135 °C
5.1: hydrogenchloride; iron / ethanol; water / 3 h / 90 °C
6.1: dichloromethane / 0.5 h / 20 °C
6.2: 20 h
7.1: triethylamine / 1,1'-bis(diphenylphosphino)ferrocene; palladium diacetate / methanol; dimethyl sulfoxide / 85 °C / 760.05 Torr
With
hydrogenchloride; ammonium acetate; iron; sodium hydride; sodium carbonate; potassium carbonate; triethylamine;
1,1'-bis(diphenylphosphino)ferrocene; palladium diacetate;
In
methanol; ethanol; dichloromethane; water; dimethyl sulfoxide; N,N-dimethyl-formamide; acetone; toluene; mineral oil;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: dichloromethane / 0.5 h / 20 °C
1.2: 20 h
2.1: triethylamine / 1,1'-bis(diphenylphosphino)ferrocene; palladium diacetate / methanol; dimethyl sulfoxide / 85 °C / 760.05 Torr
With
triethylamine;
1,1'-bis(diphenylphosphino)ferrocene; palladium diacetate;
In
methanol; dichloromethane; dimethyl sulfoxide;
