2-(2-((1-(3-methoxycarbonyl-4-methoxyphenyl)-1H-1,2,3-triazol-4-yl)methoxy)ethoxy)ethylmethanesulfonate

Base Information

Chemical Name:2-(2-((1-(3-methoxycarbonyl-4-methoxyphenyl)-1H-1,2,3-triazol-4-yl)methoxy)ethoxy)ethylmethanesulfonate
CAS No.:1609429-21-1
Molecular Formula:C₁₇H₂₃N₃O₈S
Molecular Weight:429.451
Hs Code.:

Synonyms:2-(2-((1-(3-methoxycarbonyl-4-methoxyphenyl)-1H-1,2,3-triazol-4-yl)methoxy)ethoxy)ethylmethanesulfonate

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Chemical Property of 2-(2-((1-(3-methoxycarbonyl-4-methoxyphenyl)-1H-1,2,3-triazol-4-yl)methoxy)ethoxy)ethylmethanesulfonate

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Technology Process of 2-(2-((1-(3-methoxycarbonyl-4-methoxyphenyl)-1H-1,2,3-triazol-4-yl)methoxy)ethoxy)ethylmethanesulfonate

There total 4 articles about 2-(2-((1-(3-methoxycarbonyl-4-methoxyphenyl)-1H-1,2,3-triazol-4-yl)methoxy)ethoxy)ethylmethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 943726-01-0
2-(2-(prop-2-yn-1-yloxy)ethoxy)ethyl methanesulfonate

: 845258-62-0
methyl 5-azido-2-methoxybenzoate

: 1609429-21-1
2-(2-((1-(3-methoxycarbonyl-4-methoxyphenyl)-1H-1,2,3-triazol-4-yl)methoxy)ethoxy)ethylmethanesulfonate

Guidance literature:: With bathophenanthrolinedispufonic acid disodium salt; copper(II) sulfate; sodium L-ascorbate; In water; N,N-dimethyl-formamide; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/jm5001453

Reference yield:

: 119-30-2
2-hydroxy-5-iodobenzoic acid

: 1609429-21-1
2-(2-((1-(3-methoxycarbonyl-4-methoxyphenyl)-1H-1,2,3-triazol-4-yl)methoxy)ethoxy)ethylmethanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate / acetone / Reflux; Inert atmosphere

2: sodium azide; copper(l) iodide; L-proline / N,N-dimethyl-formamide / 80 °C / Inert atmosphere

3: copper(II) sulfate; sodium L-ascorbate; bathophenanthrolinedispufonic acid disodium salt / water; N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

With copper(l) iodide; sodium azide; bathophenanthrolinedispufonic acid disodium salt; potassium carbonate; copper(II) sulfate; sodium L-ascorbate; L-proline; In water; N,N-dimethyl-formamide; acetone;
DOI:10.1021/jm5001453

Reference yield:

: 40757-09-3
methyl 2-methoxy-5-iodobenzoate

: 1609429-21-1
2-(2-((1-(3-methoxycarbonyl-4-methoxyphenyl)-1H-1,2,3-triazol-4-yl)methoxy)ethoxy)ethylmethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium azide; copper(l) iodide; L-proline / N,N-dimethyl-formamide / 80 °C / Inert atmosphere

2: copper(II) sulfate; sodium L-ascorbate; bathophenanthrolinedispufonic acid disodium salt / water; N,N-dimethyl-formamide / 0 - 20 °C / Inert atmosphere

With copper(l) iodide; sodium azide; bathophenanthrolinedispufonic acid disodium salt; copper(II) sulfate; sodium L-ascorbate; L-proline; In water; N,N-dimethyl-formamide;
DOI:10.1021/jm5001453