2-Benzyloxycarbonylamino-3-phenyl-propionic acid 2,2,2-trifluoro-ethyl ester

Base Information

Chemical Name:2-Benzyloxycarbonylamino-3-phenyl-propionic acid 2,2,2-trifluoro-ethyl ester
CAS No.:127862-78-6
Molecular Formula:C₁₉H₁₈F₃NO₄
Molecular Weight:381.351
Hs Code.:

Synonyms:2-Benzyloxycarbonylamino-3-phenyl-propionic acid 2,2,2-trifluoro-ethyl ester

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Chemical Property of 2-Benzyloxycarbonylamino-3-phenyl-propionic acid 2,2,2-trifluoro-ethyl ester

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Technology Process of 2-Benzyloxycarbonylamino-3-phenyl-propionic acid 2,2,2-trifluoro-ethyl ester

There total 1 articles about 2-Benzyloxycarbonylamino-3-phenyl-propionic acid 2,2,2-trifluoro-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 75-89-8
2,2,2-trifluoroethanol

: 3588-57-6
Z-DL-Phe-OH

: 127862-78-6
2-Benzyloxycarbonylamino-3-phenyl-propionic acid 2,2,2-trifluoro-ethyl ester

Guidance literature:: With diethylamino-sulfur trifluoride; triethylamine; In dichloromethane; at 20 ℃; for 16h; Inert atmosphere;
DOI:10.1021/acs.orglett.6b03365

Reference yield:

: 127862-78-6
2-Benzyloxycarbonylamino-3-phenyl-propionic acid 2,2,2-trifluoro-ethyl ester

: 1161-13-3,2448-45-5,3588-57-6
(R)-2-Benzyloxycarbonylamino-3-phenyl-propionic acid

Guidance literature:: With sodium hydroxide; phosphate buffer; at 25 ℃; for 47h; Yield given; porcine pancreatic lipase, pH=7.0;

Reference yield:

: 67-56-1
methanol

: 127862-78-6
2-Benzyloxycarbonylamino-3-phenyl-propionic acid 2,2,2-trifluoro-ethyl ester

: 885110-87-2
Cbz-D-Phe-OTfe

: 35909-92-3
N-carbobenzoxy-L-phenylalanine methyl ester

: 126028-14-6
2,2,2-trifluoroethyl ((benzyloxy)carbonyl)-L-phenylalaninate

: 37440-07-6
methyl (R)-2-(benzyloxycarbonylamino)-3-phenylpropanoate

Guidance literature:: With Rhizopus javanicus lipase; In di-isopropyl ether; at 25 ℃; Title compound not separated from byproducts.;
DOI:10.1139/V07-154