DICHLOROACETYL FLUORIDE

Base Information

• Chemical Name: DICHLOROACETYL FLUORIDE
• CAS No.: 359-31-9
• Molecular Formula: C2H Cl2 F O
• Molecular Weight: 130.934
• Hs Code.: 2915900090
• Mol file: 359-31-9.mol

Synonyms:Acetylfluoride, dichloro- (6CI,7CI,8CI,9CI); Dichloroacetyl fluoride

Chemical Property of DICHLOROACETYL FLUORIDE

Chemical Property:

• Boiling Point: 71°C
• PSA: 17.07000
• LogP: 1.28620

Purity/Quality:

98%min ^*data from raw suppliers

DICHLOROACETYL FLUORIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Statements: 34
• Safety Statements: 26-27-28-36/37/39

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of DICHLOROACETYL FLUORIDE

There total 3 articles about DICHLOROACETYL FLUORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

methoxyflurane (76-38-0) → methylene chloride (74-87-3) + Methyl fluoride (593-53-3) + dichloroacetyl fluoride (359-31-9) + 2,2,2-Trichloro-1,1-difluoroethyl methyl ether (661-75-6)

Guidance literature:

methoxyflurane; With potassium hydroxide; Heating;

With chlorine; at -40 ℃;

With antimonypentachloride; at 40 ℃; for 0.833333h;

DOI:10.1016/S0022-1139(98)00347-9

Reference yield:

Trichloroethylene (79-01-6) → phosgene (75-44-5) + dichloroacethyl chloride (79-36-7) + dichloroacetyl fluoride (359-31-9) + chlorofluoroacetyl chloride (359-32-0)

Guidance literature:

Produkt₅:Oxalylchlorid;Produkt₆:Pentachloraethan;Produkt₇:Hexachlorbuten;

DOI:10.1021/ja01593a039

Reference yield:

(2,2-dichloro-1,1-difluoro-ethyl)-isopropyl ether (338-16-9) → propene (187737-37-7,13987-01-4,15220-87-8,9003-07-0,676-63-1,25085-53-4) + 2-propylfluoride (420-26-8) + dichloroacetyl fluoride (359-31-9)

Guidance literature:

auf Siedetemperatur;

DOI:10.1021/ja01148a104

upstream raw materials:

(2,2-dichloro-1,1-difluoro-ethyl)-isopropyl ether

Trichloroethylene

methoxyflurane

Downstream raw materials:

hydrogen fluoride

Refernces