N-(2-methyl-1-(1-phenoxycarbonyloxy-2-methylpropan-2-ylcarbamoyl)propyl)-N-benzylacetamide

Base Information

Chemical Name:N-(2-methyl-1-(1-phenoxycarbonyloxy-2-methylpropan-2-ylcarbamoyl)propyl)-N-benzylacetamide
CAS No.:668988-22-5
Molecular Formula:C₂₅H₃₂N₂O₅
Molecular Weight:440.539
Hs Code.:

Synonyms:N-(2-methyl-1-(1-phenoxycarbonyloxy-2-methylpropan-2-ylcarbamoyl)propyl)-N-benzylacetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(2-methyl-1-(1-phenoxycarbonyloxy-2-methylpropan-2-ylcarbamoyl)propyl)-N-benzylacetamide

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Technology Process of N-(2-methyl-1-(1-phenoxycarbonyloxy-2-methylpropan-2-ylcarbamoyl)propyl)-N-benzylacetamide

There total 3 articles about N-(2-methyl-1-(1-phenoxycarbonyloxy-2-methylpropan-2-ylcarbamoyl)propyl)-N-benzylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 64-19-7,77671-22-8
acetic acid

: 78-84-2
isobutyraldehyde

: 100-46-9
benzylamine

: 288582-12-7
2-isocyano-2-methylpropyl phenyl carbonate

: 668988-22-5
N-(2-methyl-1-(1-phenoxycarbonyloxy-2-methylpropan-2-ylcarbamoyl)propyl)-N-benzylacetamide

Guidance literature:: In methanol; at 20 ℃; for 1h;
DOI:10.1055/s-2003-43355

Reference yield:

: 30093-99-3
4,4-dimethyl-2-oxazoline

: 668988-22-5
N-(2-methyl-1-(1-phenoxycarbonyloxy-2-methylpropan-2-ylcarbamoyl)propyl)-N-benzylacetamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-BuLi / tetrahydrofuran; hexane / 1 h / -78 °C

1.2: 49.7 percent / tetrahydrofuran; hexane / -78 - 20 °C

2.1: 98 percent / methanol / 1 h / 20 °C

With n-butyllithium; In tetrahydrofuran; methanol; hexane; 2.1: Ugi four-component condensation;
DOI:10.1055/s-2003-43355

Reference yield:

: 1885-14-9
phenyl chloroformate

: 668988-22-5
N-(2-methyl-1-(1-phenoxycarbonyloxy-2-methylpropan-2-ylcarbamoyl)propyl)-N-benzylacetamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-BuLi / tetrahydrofuran; hexane / 1 h / -78 °C

1.2: 49.7 percent / tetrahydrofuran; hexane / -78 - 20 °C

2.1: 98 percent / methanol / 1 h / 20 °C

With n-butyllithium; In tetrahydrofuran; methanol; hexane; 2.1: Ugi four-component condensation;
DOI:10.1055/s-2003-43355