Diethyl 2-(3-chloropropyl)-2-ethylmalonate

Base Information

Chemical Name:Diethyl 2-(3-chloropropyl)-2-ethylmalonate
CAS No.:32821-60-6
Molecular Formula:C₁₂H₂₁ClO₄
Molecular Weight:264.749
Hs Code.:2917190090
European Community (EC) Number:608-788-3
DSSTox Substance ID:DTXSID80382033
Wikidata:Q82173315
Mol file:32821-60-6.mol

Synonyms:diethyl 2-(3-chloropropyl)-2-ethylmalonate;32821-60-6;diethyl 2-(3-chloropropyl)-2-ethylpropanedioate;diethyl ethyl(3-chloropropyl)malonate;DTXSID80382033;Diethyl (3-chloropropyl)(ethyl)propanedioate;FT-0639057;A821439;diethyl 2-(3-chloranylpropyl)-2-ethyl-propanedioate;2-(3-chloropropyl)-2-ethylpropanedioic acid diethyl ester

Suppliers and Price of Diethyl 2-(3-chloropropyl)-2-ethylmalonate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
DIETHYL 2-(3-CHLOROPROPYL)-2-ETHYLMALONATE 95.00%
10G
$ 1632.36

AHH
Diethyl2-(3-chloropropyl)-2-ethylmalonate 98%
10g
$ 475.00

Total 10 raw suppliers

Chemical Property of Diethyl 2-(3-chloropropyl)-2-ethylmalonate

Chemical Property:

Vapor Pressure:0.000246mmHg at 25°C
Refractive Index:1.451
Boiling Point:324.4°C at 760 mmHg
Flash Point:115.7°C
PSA：52.60000
Density:1.08g/cm³
LogP:2.52800
XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:10
Exact Mass:264.1128368
Heavy Atom Count:17
Complexity:235

Purity/Quality:

99.9% ^*data from raw suppliers

DIETHYL 2-(3-CHLOROPROPYL)-2-ETHYLMALONATE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCC(CCCCl)(C(=O)OCC)C(=O)OCC

Technology Process of Diethyl 2-(3-chloropropyl)-2-ethylmalonate

There total 4 articles about Diethyl 2-(3-chloropropyl)-2-ethylmalonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 74-96-4
ethyl bromide

: 18719-43-2
diethyl (3-chloropropyl)malonate

: 32821-60-6
diethyl ethyl(3-chloropropyl)malonate

Guidance literature:: With tetrabutylammomium bromide; cyclohexene; In acetonitrile; at 20 ℃; Pt cathode, I = 80 mA, electrolysis;
DOI:10.1007/BF00961301

Reference yield:

: 105-53-3
diethyl malonate

: 32821-60-6
diethyl ethyl(3-chloropropyl)malonate

Guidance literature:: Multi-step reaction with 2 steps

1: 42 percent Chromat_. / cyclohexene, Bu₄NBr / acetonitrile / 20 °C / Pt cathode, I = 80 mA, electrolysis

2: 62 percent Chromat_. / cyclohexene, Bu₄NBr / acetonitrile / 20 °C / Pt cathode, I = 80 mA, electrolysis

With tetrabutylammomium bromide; cyclohexene; In acetonitrile;
DOI:10.1007/BF00961301