1-ethyl-3-methyl-4-phenyl-1,2,3-triazolium iodide

Base Information

Chemical Name:1-ethyl-3-methyl-4-phenyl-1,2,3-triazolium iodide
CAS No.:1063819-25-9
Molecular Formula:C₁₁H₁₄N₃*I
Molecular Weight:315.157
Hs Code.:

Synonyms:1-ethyl-3-methyl-4-phenyl-1,2,3-triazolium iodide

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Chemical Property of 1-ethyl-3-methyl-4-phenyl-1,2,3-triazolium iodide

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Technology Process of 1-ethyl-3-methyl-4-phenyl-1,2,3-triazolium iodide

There total 1 articles about 1-ethyl-3-methyl-4-phenyl-1,2,3-triazolium iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 103095-68-7
1-ethyl-4-phenyl-1H-1,2,3-triazole

: 74-88-4
methyl iodide

: 1063819-25-9
1-ethyl-3-methyl-4-phenyl-1,2,3-triazolium iodide

Guidance literature:: In acetonitrile; at 60 ℃; for 24h; regioselective reaction; Inert atmosphere;
DOI:10.1021/ja805781s

Reference yield: 96.0%

: 21264-30-2,90243-59-7,14592-56-4
dichloro bis(acetonitrile) palladium(II)

: 75-09-2
dichloromethane

: 1063819-25-9
1-ethyl-3-methyl-4-phenyl-1,2,3-triazolium iodide

: [PdCl₂(C₂N₃(CH₃)(C₂H₅)C₆H₅)2]*0.25CH₂Cl₂

Guidance literature:: With Ag₂O; In dichloromethane; (C2HN3(CH3)(C2H5)C6H5)I and Ag2O in CH2Cl2 stirred at room temp. for 24 h, filtered, Pd complex added, stirred at room temp. for 2 h; filtered, eluted (SiO2, CH2Cl2), evapd., washed (pentane); obtained as an 1/6 mixt. of isomers; elem. anal.;
DOI:10.1021/om101076u