(Z)-5,6-dihydrodibenzo[b,f]azocine

Base Information

• Chemical Name: (Z)-5,6-dihydrodibenzo[b,f]azocine
• CAS No.: 23194-93-6
• Molecular Formula: C₁₅H₁₃N
• Molecular Weight: 207.275
• Hs Code.: 29339900
• Mol file: 23194-93-6.mol

Synonyms:2-azatricyclo[10.4.0.0^4,9]hexadeca-1⁽¹⁶⁾,4⁽⁹⁾,5,7,10,12,14-heptene

Chemical Property of (Z)-5,6-dihydrodibenzo[b,f]azocine

Chemical Property:

• Melting Point: 108-109 °C
• Boiling Point: 378.3±37.0 °C(Predicted)
• PKA: 4.44±0.20(Predicted)
• Density: 1.085±0.06 g/cm3(Predicted)

Purity/Quality:

97% ^*data from raw suppliers

5,6-Dihydrodibenz[b,f]azocine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Uses: 5,6-Dihydrodibenz[b,f]azocine is an intermediate used in the synthesis of strained cyclooctyne derivatives.

Technology Process of (Z)-5,6-dihydrodibenzo[b,f]azocine

There total 25 articles about (Z)-5,6-dihydrodibenzo[b,f]azocine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

tert-butyl {2-[(Z)-2-(2-formylphenyl)ethenyl]phenyl}carbamate (1207355-24-5) → (Z)-5,6-dihydrodibenzo[b,f]azocine (23194-93-6)

Guidance literature:

tert-butyl {2-[(Z)-2-(2-formylphenyl)ethenyl]phenyl}carbamate; With hydrogenchloride; In ethyl acetate; at 20 ℃; for 1h;

With sodium tetrahydroborate; water; In ethyl acetate; at 20 ℃;

DOI:10.1039/b917797c

Reference yield: 96.0%

dibenzo[b,f]azocin-6(5H)-one (23112-88-1) → 2-azatricyclo[10.4.0.04,9]hexadeca-1(16),4(9),5,7,10,12,14-heptene (23194-93-6)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; at 35 ℃; for 24h; Inert atmosphere; Sealed tube;

DOI:10.1021/acs.oprd.9b00406

Reference yield: 91.0%

5,6,11,12-tetrahydrodibenz[b,f]azocin-6-one (6047-29-6) → 2-azatricyclo[10.4.0.04,9]hexadeca-1(16),4(9),5,7,10,12,14-heptene (23194-93-6)

Guidance literature:

With lithium aluminium tetrahydride; In diethyl ether; at 35 ℃; for 15h; Inert atmosphere;

DOI:10.1055/s-0033-1340509

upstream raw materials:

tert-butyl {2-[(Z)-2-(2-formylphenyl)ethenyl]phenyl}carbamate

dibenzo[b,f]azocin-6(5H)-one

N-[tricyclo[9.4.0.0^3,8]pentadeca-1⁽¹¹⁾,3,5,7,9,12,14-heptaen-2-ylidene]hydroxylamine

dibenzosuberenon

Downstream raw materials:

N-(3-aminopropionyl)-5,6-dihydro-11,12-didehydrodibenzo[b,f]azocine

DBCO-4PEG-biotin

N-boc protected ADIBO-PEG₄-amine

DBCO-PEG₄-amine

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