(Z)-methyl 3-(2,3-dichlorophenyl)-2-(2-methyl-1,3-dioxolan-2-yl)acrylate

Base Information

Chemical Name:(Z)-methyl 3-(2,3-dichlorophenyl)-2-(2-methyl-1,3-dioxolan-2-yl)acrylate
CAS No.:1376615-40-5
Molecular Formula:C₁₄H₁₄Cl₂O₄
Molecular Weight:317.169
Hs Code.:

Synonyms:(Z)-methyl 3-(2,3-dichlorophenyl)-2-(2-methyl-1,3-dioxolan-2-yl)acrylate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-methyl 3-(2,3-dichlorophenyl)-2-(2-methyl-1,3-dioxolan-2-yl)acrylate

Chemical Property:

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Technology Process of (Z)-methyl 3-(2,3-dichlorophenyl)-2-(2-methyl-1,3-dioxolan-2-yl)acrylate

There total 4 articles about (Z)-methyl 3-(2,3-dichlorophenyl)-2-(2-methyl-1,3-dioxolan-2-yl)acrylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 107-21-1
ethylene glycol

: 68064-69-7
(Z)-methyl 2-(2,3-dichlorobenzylidene)-3-oxobutanoate

: 1376615-40-5
(Z)-methyl 3-(2,3-dichlorophenyl)-2-(2-methyl-1,3-dioxolan-2-yl)acrylate

Guidance literature:: With toluene-4-sulfonic acid; In toluene; for 6h; Reflux;

Reference yield:

: 105-45-3
acetoacetic acid methyl ester

: 1376615-40-5
(Z)-methyl 3-(2,3-dichlorophenyl)-2-(2-methyl-1,3-dioxolan-2-yl)acrylate

Guidance literature:: Multi-step reaction with 2 steps

1: piperidine; 2-Picolinic acid / isopropyl alcohol / 45 °C

2: toluene-4-sulfonic acid / toluene / 6 h / Dean-Stark; Reflux

With piperidine; 2-Picolinic acid; toluene-4-sulfonic acid; In isopropyl alcohol; toluene;

Reference yield:

: 6334-18-5
2,3-dichlorobenzylaldehyde

: 1376615-40-5
(Z)-methyl 3-(2,3-dichlorophenyl)-2-(2-methyl-1,3-dioxolan-2-yl)acrylate

Guidance literature:: Multi-step reaction with 2 steps

1: piperidine; 2-Picolinic acid / isopropyl alcohol / 45 °C

2: toluene-4-sulfonic acid / toluene / 6 h / Dean-Stark; Reflux

With piperidine; 2-Picolinic acid; toluene-4-sulfonic acid; In isopropyl alcohol; toluene;