METHYL 2,6-DICHLOROBENZOATE

Base Information

• Chemical Name: METHYL 2,6-DICHLOROBENZOATE
• CAS No.: 14920-87-7
• Molecular Formula: C8H6Cl2O2
• Molecular Weight: 205.04
• Hs Code.: 2916399090
• Mol file: 14920-87-7.mol

Synonyms:2,6-Dichlorobenzoic acid methyl ester;

Chemical Property of METHYL 2,6-DICHLOROBENZOATE

Chemical Property:

• Vapor Pressure: 0.0113mmHg at 25°C
• Melting Point: 25-30 °C
• Refractive Index: 1.545
• Boiling Point: 261.8 °C at 760 mmHg
• Flash Point: 111.2 °C
• PSA: 26.30000
• Density: 1.355 g/cm³
• LogP: 2.78000

Purity/Quality:

97% ^*data from raw suppliers

Methyl2,6-Dichlorobenzoate ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi
• Safety Statements: 22-24/25

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of METHYL 2,6-DICHLOROBENZOATE

There total 15 articles about METHYL 2,6-DICHLOROBENZOATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

carbonic acid dimethyl ester (616-38-6) + 2,6-dichlorobenzoic acid (50-30-6) → 2,6-dichlorobenzoic acid methyl ester (14920-87-7)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; for 24h; Heating;

DOI:10.1021/jo011036s

Reference yield: 83.0%

4-bromo-2-chloro-6-fluorobenzoic acid (1321613-01-7) + methyl iodide (74-88-4) → 2,6-dichlorobenzoic acid methyl ester (14920-87-7)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

Reference yield: 79.0%

methanol (67-56-1) + 2,6-dichlorobenzaldehyde (83-38-5) → 2,6-dichlorobenzoic acid methyl ester (14920-87-7)

Guidance literature:

With manganese(IV) oxide; caesium carbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; 1-butyl-3-methylimidazolium Tetrafluoroborate; at 20 ℃; for 24h; Inert atmosphere;

DOI:10.1016/j.tet.2013.06.014

upstream raw materials:

N-(2,6-dichlorobenzoyl)-N'-(4-chlorophenyl)-urea

sodium methylate

2,6-Dichlorobenzoyl chloride

trimethylsulphonium hydroxide

Downstream raw materials:

methyl chlorobenzoate

3-(2',6'-dichlorophenyl)-3-oxopropionitrile

methyl 2,6-dichloro-4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzoate

2,6-dichlorobenzyl alcohol

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