3-(Benzoylamino)-1-methylimidazolium hydroxide inner salt

Base Information

• Chemical Name: 3-(Benzoylamino)-1-methylimidazolium hydroxide inner salt
• CAS No.: 54558-36-0
• Molecular Formula: C₁₁H₁₁N₃O
• Molecular Weight: 201.228
• Mol file: 54558-36-0.mol

Synonyms:3-(Benzoylamino)-1-methylimidazolium hydroxide inner salt

Chemical Property of 3-(Benzoylamino)-1-methylimidazolium hydroxide inner salt

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-(Benzoylamino)-1-methylimidazolium hydroxide inner salt

There total 1 articles about 3-(Benzoylamino)-1-methylimidazolium hydroxide inner salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

benzoyl chloride (98-88-4) + 1-amino-3-methyl-3H-imidazol-1-ium mesitylenesulfonate → 3-(Benzoylamino)-1-methylimidazolium hydroxide inner salt (54558-36-0)

Guidance literature:

With potassium carbonate; In dichloromethane; for 6h; Heating;

DOI:10.1021/jo00073a059

Reference yield: 95.0%

3-(Benzoylamino)-1-methylimidazolium hydroxide inner salt (54558-36-0) + methyl iodide (74-88-4) → 1-(benzoylmethylamino)-3-methyl-3H-imidazol-1-ium iodide

Guidance literature:

In ethyl acetate; for 24h; Ambient temperature;

DOI:10.1021/jo00073a059

Reference yield:

3-(Benzoylamino)-1-methylimidazolium hydroxide inner salt (54558-36-0) → 1-phenyl-propan-1-one (93-55-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 95 percent / ethyl acetate / 24 h / Ambient temperature

2: 87 percent / tetrahydrofuran / -78 deg C to room temp. then room temp., 45 min

In tetrahydrofuran; ethyl acetate;

DOI:10.1021/jo00073a059

upstream raw materials:

benzoyl chloride

Downstream raw materials:

benzophenone

phenyl butyl ketone

acetophenone

1-phenyl-propan-1-one