methyl 4-(6-phenyl-1,4-dioxaspiro[4.5]decan-6-yl)butanoate

Base Information

Chemical Name:methyl 4-(6-phenyl-1,4-dioxaspiro[4.5]decan-6-yl)butanoate
CAS No.:1356465-25-2
Molecular Formula:C₁₉H₂₆O₄
Molecular Weight:318.413
Hs Code.:

Synonyms:methyl 4-(6-phenyl-1,4-dioxaspiro[4.5]decan-6-yl)butanoate

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Chemical Property of methyl 4-(6-phenyl-1,4-dioxaspiro[4.5]decan-6-yl)butanoate

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Technology Process of methyl 4-(6-phenyl-1,4-dioxaspiro[4.5]decan-6-yl)butanoate

There total 5 articles about methyl 4-(6-phenyl-1,4-dioxaspiro[4.5]decan-6-yl)butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1356465-24-1
(E)-methyl 4-(6-phenyl-1,4-dioxaspiro[4.5]decan-6-yl)but-2-enoate

: 1356465-25-2
methyl 4-(6-phenyl-1,4-dioxaspiro[4.5]decan-6-yl)butanoate

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In methanol; for 3.5h; under 1292.9 Torr;

Reference yield:

: 1444-65-1
(RS)-2-phenylcyclohexanone

: 1356465-25-2
methyl 4-(6-phenyl-1,4-dioxaspiro[4.5]decan-6-yl)butanoate

Guidance literature:: Multi-step reaction with 5 steps

1.1: sodium hexamethyldisilazane / 1,2-dimethoxyethane / 0.33 h / Cooling with ice

1.2: 0.33 h / 20 °C

1.3: 2 h / 20 °C

2.1: toluene-4-sulfonic acid / benzene / 16.5 h / Reflux

3.1: sodium periodate / osmium(VIII) oxide / water; tert-butyl alcohol / 3 h

4.1: tetrahydrofuran / 18 h / Reflux

5.1: hydrogen / palladium 10% on activated carbon / methanol / 3.5 h / 1292.9 Torr

With sodium periodate; hydrogen; sodium hexamethyldisilazane; toluene-4-sulfonic acid; osmium(VIII) oxide; palladium 10% on activated carbon; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; water; tert-butyl alcohol; benzene;

Reference yield:

: 7079-07-4
2-allyl-2-phenylcyclohexan-1-one

: 1356465-25-2
methyl 4-(6-phenyl-1,4-dioxaspiro[4.5]decan-6-yl)butanoate

Guidance literature:: Multi-step reaction with 4 steps

1: toluene-4-sulfonic acid / benzene / 16.5 h / Reflux

2: sodium periodate / osmium(VIII) oxide / water; tert-butyl alcohol / 3 h

3: tetrahydrofuran / 18 h / Reflux

4: hydrogen / palladium 10% on activated carbon / methanol / 3.5 h / 1292.9 Torr

With sodium periodate; hydrogen; toluene-4-sulfonic acid; osmium(VIII) oxide; palladium 10% on activated carbon; In tetrahydrofuran; methanol; water; tert-butyl alcohol; benzene;