N¹-(4-bromo-2,6-diisopropylphenyl)-N²-(2,6-diisopropylphenyl)-oxalamide

Base Information

Chemical Name:N¹-(4-bromo-2,6-diisopropylphenyl)-N²-(2,6-diisopropylphenyl)-oxalamide
CAS No.:1643961-87-8
Molecular Formula:C₂₆H₃₅BrN₂O₂
Molecular Weight:487.48
Hs Code.:

N<SUP>1</SUP>-(4-bromo-2,6-diisopropylphenyl)-N<SUP>2</SUP>-(2,6-diisopropylphenyl)-oxalamide

Synonyms:N¹-(4-bromo-2,6-diisopropylphenyl)-N²-(2,6-diisopropylphenyl)-oxalamide

Suppliers and Price of N¹-(4-bromo-2,6-diisopropylphenyl)-N²-(2,6-diisopropylphenyl)-oxalamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of N¹-(4-bromo-2,6-diisopropylphenyl)-N²-(2,6-diisopropylphenyl)-oxalamide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of N¹-(4-bromo-2,6-diisopropylphenyl)-N²-(2,6-diisopropylphenyl)-oxalamide

There total 3 articles about N¹-(4-bromo-2,6-diisopropylphenyl)-N²-(2,6-diisopropylphenyl)-oxalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 79-37-8
oxalyl dichloride

: 80058-84-0
4-bromo-2,6-diisopropylaniline

: 169772-26-3
2-[(2,6-diisopropylphenyl)amino]-2-oxoacetic acid

: 1643961-87-8
N¹-(4-bromo-2,6-diisopropylphenyl)-N²-(2,6-diisopropylphenyl)-oxalamide

Guidance literature:: oxalyl dichloride; 2-[(2,6-diisopropylphenyl)amino]-2-oxoacetic acid; In dichloromethane; N,N-dimethyl-formamide; at 20 ℃; for 4h;

4-bromo-2,6-diisopropylaniline; With triethylamine; In dichloromethane;
DOI:10.1002/ejoc.201402364

Reference yield: 53.0%

: 2-((2,6-diisopropylphenyl)amino)-2-oxoacetyl chloride

: 80058-84-0
4-bromo-2,6-diisopropylaniline

: 1643961-87-8
N¹-(4-bromo-2,6-diisopropylphenyl)-N²-(2,6-diisopropylphenyl)-oxalamide

Guidance literature:: With triethylamine; In dichloromethane; at 0 - 25 ℃; for 15.1667h; Schlenk technique; Inert atmosphere;
DOI:10.1002/chem.201502381

Reference yield:

: 24544-04-5
2,6-diisopropylbenzenamine

: 1643961-87-8
N¹-(4-bromo-2,6-diisopropylphenyl)-N²-(2,6-diisopropylphenyl)-oxalamide

Guidance literature:: Multi-step reaction with 2 steps

1: bromine / dichloromethane; methanol / 25.5 h / 25 °C / Schlenk technique; Inert atmosphere

2: triethylamine / dichloromethane / 15.17 h / 0 - 25 °C / Schlenk technique; Inert atmosphere

With bromine; triethylamine; In methanol; dichloromethane;
DOI:10.1002/chem.201502381