thioyl chloride

Base Information

• Chemical Name: thioyl chloride
• CAS No.: 14989-32-3
• Molecular Formula: ClS
• Molecular Weight: 68.5269
• Mol file: 14989-32-3.mol

Synonyms:thioyl chloride

Chemical Property of thioyl chloride

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of thioyl chloride

There total 7 articles about thioyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

trichlorothiophosphine (3982-91-0) + dinitrogen monoxide (10024-97-2) → sulphur monochloride (14989-32-3) + PSCl2(1+) (52826-97-8) + PSCl3(1+) + PCl2(1+) (75601-84-2) + clorine (14700-96-0,14835-24-6,15723-23-6,16547-50-5,16885-04-4,16887-00-6,16904-11-3,16904-12-4,16999-02-3,20337-89-7,20499-73-4,22537-15-1,22537-27-5,22541-73-7,22541-74-8,24203-47-2,33944-49-9,34937-26-3,37352-90-2)

Guidance literature:

In gas; High Pressure; the reagent ions were generated in an electron impact high-pressure ion source contg. N2O; the reagent ions were selected using a quadrupole mass filter before being injected into a drift region contg. helium carriergas; at 298 K; monitoring by quadrupole mass spectrometer at the end of the flow tube; Kinetics;

DOI:10.1016/j.chemphys.2004.03.033

Reference yield: 93.0%

trichlorothiophosphine (3982-91-0) + carbon monoxide (201230-82-2) → sulphur monochloride (14989-32-3) + PSCl2(1+) (52826-97-8) + PSCl3(1+) + PCl2(1+) (75601-84-2) + clorine (14700-96-0,14835-24-6,15723-23-6,16547-50-5,16885-04-4,16887-00-6,16904-11-3,16904-12-4,16999-02-3,20337-89-7,20499-73-4,22537-15-1,22537-27-5,22541-73-7,22541-74-8,24203-47-2,33944-49-9,34937-26-3,37352-90-2)

Guidance literature:

In gas; High Pressure; the reagent ions were generated in an electron impact high-pressure ion source contg. CO; the reagent ions were selected using a quadrupole massfilter before being injected into a drift region contg. helium carrier gas; at 298 K; monitoring by quadrupole mass spectrometer at the end of the flow tube; Kinetics;

DOI:10.1016/j.chemphys.2004.03.033

Reference yield:

mercapto radical (7704-34-9) + chlorine (7782-50-5) → thioyl chloride (14989-32-3) + clorine (14700-96-0,14835-24-6,15723-23-6,16547-50-5,16885-04-4,16887-00-6,16904-11-3,16904-12-4,16999-02-3,20337-89-7,20499-73-4,22537-15-1,22537-27-5,22541-73-7,22541-74-8,24203-47-2,33944-49-9,34937-26-3,37352-90-2)

Guidance literature:

In gaseous matrix; other Radiation; laser initiated reaction (laser fluence< 2E-4 J/cm**2, Ar buffer gas, ratio Ar/Cl2/H2S 200:40:1, total pressure 10 Torr); not isolated; infrared chemiluminescence monitoring; Kinetics;

DOI:10.1063/1.439284

upstream raw materials:

hydrogen sulfide

chlorine

mercapto radical

carbon oxide sulfide

Downstream raw materials:

3-cyclopentyloxy-4-methoxy benzoic acid chloride

1-benzoyl-4-chloro-3-(3-chloro-1,2,5-thiadiazol-4-yl)-1,2,5,6-tetrahydropyridine

sulfur dichloride

disulfur