tantalum thiochloride

Base Information

Chemical Name:tantalum thiochloride
CAS No.:60994-01-6
Molecular Formula:Cl₃STa
Molecular Weight:319.373
Hs Code.:

Synonyms:tantalum thiochloride

Suppliers and Price of tantalum thiochloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of tantalum thiochloride

Chemical Property:

Purity/Quality:

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Technology Process of tantalum thiochloride

There total 3 articles about tantalum thiochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: antimony(III) sulfide

: 7721-01-9
tantalum pentachloride

: 10025-91-9
antimony(III) chloride

: 60994-01-6
tantalum thiochloride

Guidance literature:: With CS₂; In carbon disulfide; TaCl5 was placed in ampoule under a stream of N2, ampoule was evacuated, left to pump for 0.5 h, Sb2S3 was pumped at 200°C overnight, CS2 was distilled into ampoule, cooled to liq. N2 temp., solvent was added, stirred at room temp. for 3 d; ampoule quickly opened under N2, filtered on vac. line, ppt. was washedwith CS2, pumped for 24 h; elem. anal.;
DOI:10.1039/DT9840000845

Reference yield:

: diboron trisulfide

: 7721-01-9
tantalum pentachloride

: 10294-34-5
boron trichloride

: 60994-01-6
tantalum thiochloride

Guidance literature:: 80°C; beginning of react. at room temp.;
DOI:10.1016/0022-5088(77)90115-1

Reference yield:

: 3385-94-2
hexamethyldisilathiane

: 7721-01-9
tantalum pentachloride

: 75-77-4
chloro-trimethyl-silane

: 60994-01-6
tantalum thiochloride

Guidance literature:: In dichloromethane; (vac. or Ar atmosphere) dropwise addn. of soln. of (Me3Si)2S (-30°C) to suspn. of metal compound (-78°C), stirring, warming to room temp.; high yield;
DOI:10.1016/S0277-5387(00)80757-3