(2E)-1-Methyl-2-[(3-methylphenyl)methylidene]-1-phenylhydrazine

Base Information

Chemical Name:(2E)-1-Methyl-2-[(3-methylphenyl)methylidene]-1-phenylhydrazine
CAS No.:59670-14-3
Molecular Formula:C15H16 N2
Molecular Weight:224.3009
Hs Code.:
DSSTox Substance ID:DTXSID40421917

Synonyms:DTXSID40421917;(2E)-1-Methyl-2-[(3-methylphenyl)methylidene]-1-phenylhydrazine

Suppliers and Price of (2E)-1-Methyl-2-[(3-methylphenyl)methylidene]-1-phenylhydrazine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of (2E)-1-Methyl-2-[(3-methylphenyl)methylidene]-1-phenylhydrazine

Chemical Property:

Vapor Pressure:5.23E-05mmHg at 25°C
Boiling Point:347.9°C at 760 mmHg
Flash Point:164.2°C
Density:0.97g/cm³
XLogP3:4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:224.131348519
Heavy Atom Count:17
Complexity:243

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=CC=C1)C=NN(C)C2=CC=CC=C2
Isomeric SMILES:CC1=CC(=CC=C1)/C=N/N(C)C2=CC=CC=C2

Technology Process of (2E)-1-Methyl-2-[(3-methylphenyl)methylidene]-1-phenylhydrazine

There total 3 articles about (2E)-1-Methyl-2-[(3-methylphenyl)methylidene]-1-phenylhydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 59670-13-2
C₁₄H₁₄N₂

: 74-88-4
methyl iodide

: 59670-14-3
N-Methyl-N-phenyl-N'-[1-m-tolyl-meth-(E)-ylidene]-hydrazine

Guidance literature:: C₁₄H₁₄N₂; With sodium hydride; In tetrahydrofuran; at 0 ℃; for 0.25h; Inert atmosphere;

methyl iodide; In tetrahydrofuran; at 25 ℃; for 5h; Inert atmosphere;
DOI:10.1021/acs.orglett.6b02711

Reference yield:

: 100-63-0
phenylhydrazine

: 59670-14-3
N-Methyl-N-phenyl-N'-[1-m-tolyl-meth-(E)-ylidene]-hydrazine

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetic acid / ethanol / 0 °C / Inert atmosphere; Reflux

2.1: sodium hydride / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere

2.2: 5 h / 25 °C / Inert atmosphere

With sodium hydride; acetic acid; In tetrahydrofuran; ethanol;
DOI:10.1021/acs.orglett.6b02711