1,1,1-triphenyl-2,1λ(5)-benzoxabismol-3(1H)-one

Base Information

Chemical Name:1,1,1-triphenyl-2,1λ(5)-benzoxabismol-3(1H)-one
CAS No.:105242-73-7
Molecular Formula:C₂₅H₁₉BiO₂
Molecular Weight:560.405
Hs Code.:

Synonyms:1,1,1-triphenyl-2,1λ(5)-benzoxabismol-3(1H)-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,1,1-triphenyl-2,1λ(5)-benzoxabismol-3(1H)-one

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Technology Process of 1,1,1-triphenyl-2,1λ(5)-benzoxabismol-3(1H)-one

There total 1 articles about 1,1,1-triphenyl-2,1λ(5)-benzoxabismol-3(1H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 3049-07-8
pentaphenylbismuth

: 105242-73-7
1,1,1-triphenyl-2,1λ(5)-benzoxabismol-3(1H)-one

: 71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1
benzene

Guidance literature:: With carbon dioxide; In toluene; Under Ar, cooling of soln. to -20°C, passing of CO2 through the soln for 10 h.; Warming to room temp., evapn. of solvent in vac., benzene determined byGC, washing of colourless residue with petroleum ether, dissolving in benzene, filtn., concg., elem. anal.;

Reference yield: 78.0%

: 105242-73-7
1,1,1-triphenyl-2,1λ(5)-benzoxabismol-3(1H)-one

: 603-33-8
triphenylbismuthane

: 71-43-2,26181-88-4,54682-86-9,13967-78-7,174973-66-1
benzene

Guidance literature:: byproducts: CO2; Heating at 120°C for 1 h under Ar.;

Reference yield: 67.0%

: 105242-73-7
1,1,1-triphenyl-2,1λ(5)-benzoxabismol-3(1H)-one

: 603-36-1
triphenylantimony

: 16894-68-1
tetraphenylchloroantimony(V)

Guidance literature:: Addn. of Bi-compound to a melt of Ph3Sb at 60°C with stirring, slow heating to 120°C, keeping the temp. for 1 h.; Cooling to room temp., washing (petroleum ether), treatment of residue with aq. HCl, refluxing (15 min), filtn., concg., recrystn. (H2O).;