3-fluorophenyl(phenyl)carbamic chloride

Base Information

Chemical Name:3-fluorophenyl(phenyl)carbamic chloride
CAS No.:129622-62-4
Molecular Formula:C₁₃H₉ClFNO
Molecular Weight:249.672
Hs Code.:

Synonyms:3-fluorophenyl(phenyl)carbamic chloride

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Chemical Property of 3-fluorophenyl(phenyl)carbamic chloride

Chemical Property:

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Technology Process of 3-fluorophenyl(phenyl)carbamic chloride

There total 7 articles about 3-fluorophenyl(phenyl)carbamic chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 32315-10-9
bis(trichloromethyl) carbonate

: 500-41-4
3-fluoro-N-phenyl-aniline

: 129622-62-4
3-fluorophenyl(phenyl)carbamic chloride

Guidance literature:: With pyridine; In dichloromethane; at 0 - 25 ℃; Inert atmosphere; Large scale;
DOI:10.1021/acs.jmedchem.6b00871

Reference yield:

: 372-19-0
meta-fluoroaniline

: 129622-62-4
3-fluorophenyl(phenyl)carbamic chloride

Guidance literature:: Multi-step reaction with 2 steps

1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; sodium t-butanolate / toluene / 3 h / 105 °C / Large scale

2: pyridine / dichloromethane / 0 - 25 °C / Inert atmosphere; Large scale

With pyridine; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; sodium t-butanolate; In dichloromethane; toluene;
DOI:10.1021/acs.jmedchem.6b00871

Reference yield:

: 108-86-1,52753-63-6
bromobenzene

: 129622-62-4
3-fluorophenyl(phenyl)carbamic chloride

Guidance literature:: Multi-step reaction with 2 steps

1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; sodium t-butanolate / toluene / 3 h / 105 °C / Large scale

2: pyridine / dichloromethane / 0 - 25 °C / Inert atmosphere; Large scale

With pyridine; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; sodium t-butanolate; In dichloromethane; toluene;
DOI:10.1021/acs.jmedchem.6b00871