1-(4-cyano-phenyl)-3-(4-methoxy-phenyl)-1-methyl-3-((Z)-1-phenyl-propenyl)-urea

Base Information

Chemical Name:1-(4-cyano-phenyl)-3-(4-methoxy-phenyl)-1-methyl-3-((Z)-1-phenyl-propenyl)-urea
CAS No.:1256930-07-0
Molecular Formula:C₂₅H₂₃N₃O₂
Molecular Weight:397.477
Hs Code.:

Synonyms:1-(4-cyano-phenyl)-3-(4-methoxy-phenyl)-1-methyl-3-((Z)-1-phenyl-propenyl)-urea

Suppliers and Price of 1-(4-cyano-phenyl)-3-(4-methoxy-phenyl)-1-methyl-3-((Z)-1-phenyl-propenyl)-urea

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(4-cyano-phenyl)-3-(4-methoxy-phenyl)-1-methyl-3-((Z)-1-phenyl-propenyl)-urea

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 1-(4-cyano-phenyl)-3-(4-methoxy-phenyl)-1-methyl-3-((Z)-1-phenyl-propenyl)-urea

There total 5 articles about 1-(4-cyano-phenyl)-3-(4-methoxy-phenyl)-1-methyl-3-((Z)-1-phenyl-propenyl)-urea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 623-00-7
4-bromobenzenecarbonitrile

: 1256929-96-0
1-(4-methoxyphenyl)-3-methyl-1-((Z)-1-phenylpropenyl)urea

: 1256930-07-0
1-(4-cyano-phenyl)-3-(4-methoxy-phenyl)-1-methyl-3-((Z)-1-phenyl-propenyl)-urea

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; sodium t-butanolate; In toluene; at 110 ℃; for 48h; Inert atmosphere;
DOI:10.1021/ol102155h

Reference yield:

: 1256930-33-2
1-(4-cyanophenyl)-3-(4-methoxyphenyl)-1-methyl-3-(1-phenylallyl)urea

: 1256930-07-0
1-(4-cyano-phenyl)-3-(4-methoxy-phenyl)-1-methyl-3-((Z)-1-phenyl-propenyl)-urea

: 1261161-62-9
1-(4-cyano-phenyl)-3-(4-methoxy-phenyl)-1-methyl-3-((E)-1-phenyl-propenyl)-urea

Guidance literature:: With (carbonyl)(chloro)(hydrido)tris(triphenylphosphine)ruthenium(II); at 70 ℃; optical yield given as %de;
DOI:10.1021/ol102155h

Reference yield:

: C₂₄H₂₁N₃O₂

: 74-88-4
methyl iodide

: 1256930-07-0
1-(4-cyano-phenyl)-3-(4-methoxy-phenyl)-1-methyl-3-((Z)-1-phenyl-propenyl)-urea

Guidance literature:: C₂₄H₂₁N₃O₂; With sodium hydride; In N,N-dimethyl-formamide; mineral oil; at 0 ℃; for 0.5h; Inert atmosphere;

methyl iodide; In N,N-dimethyl-formamide; mineral oil; at 0 - 20 ℃; optical yield given as %de; Inert atmosphere;
DOI:10.1021/ol1027442