Allyl-2-acetamido-2-desoxy-6-O-(4-methoxybenzyl)-3-O-(methoxymethyl)-4-O<(methylthio)thiocarbonyl>-α-D-glucopyranosid

Base Information

Chemical Name:Allyl-2-acetamido-2-desoxy-6-O-(4-methoxybenzyl)-3-O-(methoxymethyl)-4-O<(methylthio)thiocarbonyl>-α-D-glucopyranosid
CAS No.:136408-93-0
Molecular Formula:C₂₃H₃₃NO₈S₂
Molecular Weight:515.649
Hs Code.:

Synonyms:Allyl-2-acetamido-2-desoxy-6-O-(4-methoxybenzyl)-3-O-(methoxymethyl)-4-O<(methylthio)thiocarbonyl>-α-D-glucopyranosid

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Chemical Property of Allyl-2-acetamido-2-desoxy-6-O-(4-methoxybenzyl)-3-O-(methoxymethyl)-4-O<(methylthio)thiocarbonyl>-α-D-glucopyranosid

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Technology Process of Allyl-2-acetamido-2-desoxy-6-O-(4-methoxybenzyl)-3-O-(methoxymethyl)-4-O<(methylthio)thiocarbonyl>-α-D-glucopyranosid

There total 6 articles about Allyl-2-acetamido-2-desoxy-6-O-(4-methoxybenzyl)-3-O-(methoxymethyl)-4-O<(methylthio)thiocarbonyl>-α-D-glucopyranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 54400-75-8
allyl 2-acetamido-2-deoxy-α-D-glucopyranoside

: 136408-93-0
Allyl-2-acetamido-2-desoxy-6-O-(4-methoxybenzyl)-3-O-(methoxymethyl)-4-O<(methylthio)thiocarbonyl>-α-D-glucopyranosid

Guidance literature:: Multi-step reaction with 4 steps

1: 91 percent / CSA / acetonitrile / 0.5 h

2: 83 percent / 2,6-lutidine / acetonitrile / 16 h / Heating

3: 79 percent / NaBH₃CN, molecular sieve 3 Angstroem, trifluoroacetic acid / tetrahydrofuran / 0 °C

4: 1) 5 N NaOH / 1) 5 deg C, 30 min., 2) 1 h

With 2,6-dimethylpyridine; sodium hydroxide; 3 A molecular sieve; camphor-10-sulfonic acid; sodium cyanoborohydride; trifluoroacetic acid; In tetrahydrofuran; acetonitrile;

Reference yield:

: 2186-92-7
p-Anisaldehyde dimethyl acetal

: 136408-93-0
Allyl-2-acetamido-2-desoxy-6-O-(4-methoxybenzyl)-3-O-(methoxymethyl)-4-O<(methylthio)thiocarbonyl>-α-D-glucopyranosid

Guidance literature:: Multi-step reaction with 4 steps

1: 91 percent / CSA / acetonitrile / 0.5 h

2: 83 percent / 2,6-lutidine / acetonitrile / 16 h / Heating

3: 79 percent / NaBH₃CN, molecular sieve 3 Angstroem, trifluoroacetic acid / tetrahydrofuran / 0 °C

4: 1) 5 N NaOH / 1) 5 deg C, 30 min., 2) 1 h

With 2,6-dimethylpyridine; sodium hydroxide; 3 A molecular sieve; camphor-10-sulfonic acid; sodium cyanoborohydride; trifluoroacetic acid; In tetrahydrofuran; acetonitrile;

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 136408-93-0
Allyl-2-acetamido-2-desoxy-6-O-(4-methoxybenzyl)-3-O-(methoxymethyl)-4-O<(methylthio)thiocarbonyl>-α-D-glucopyranosid

Guidance literature:: Multi-step reaction with 4 steps

1: 80 percent / HC(OCH₃)3, CSA / dimethylformamide / 6 h

2: 83 percent / 2,6-lutidine / acetonitrile / 16 h / Heating

3: 79 percent / NaBH₃CN, molecular sieve 3 Angstroem, trifluoroacetic acid / tetrahydrofuran / 0 °C

4: 1) 5 N NaOH / 1) 5 deg C, 30 min., 2) 1 h

With 2,6-dimethylpyridine; sodium hydroxide; 3 A molecular sieve; camphor-10-sulfonic acid; sodium cyanoborohydride; trifluoroacetic acid; trimethyl orthoformate; In tetrahydrofuran; N,N-dimethyl-formamide; acetonitrile;