7-(4'-methoxy)phenyl-5,6,8,9-tetrahydroquino<8,7-b><1,10>phenanthroline

Base Information

Chemical Name:7-(4'-methoxy)phenyl-5,6,8,9-tetrahydroquino<8,7-b><1,10>phenanthroline
CAS No.:148066-20-0
Molecular Formula:C₂₆H₂₁N₃O
Molecular Weight:391.472
Hs Code.:

Synonyms:7-(4'-methoxy)phenyl-5,6,8,9-tetrahydroquino<8,7-b><1,10>phenanthroline

Suppliers and Price of 7-(4'-methoxy)phenyl-5,6,8,9-tetrahydroquino<8,7-b><1,10>phenanthroline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 7-(4'-methoxy)phenyl-5,6,8,9-tetrahydroquino<8,7-b><1,10>phenanthroline

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 7-(4'-methoxy)phenyl-5,6,8,9-tetrahydroquino<8,7-b><1,10>phenanthroline

There total 2 articles about 7-(4'-methoxy)phenyl-5,6,8,9-tetrahydroquino<8,7-b><1,10>phenanthroline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 56826-69-8
5,6,7,8-tetrahydro-8-quinolinone

: N,N-dimethyl-4'-(methoxy)benzylidene ammonium chloride

: 148066-20-0
7-(4'-methoxy)phenyl-5,6,8,9-tetrahydroquino<8,7-b><1,10>phenanthroline

Guidance literature:: 5,6,7,8-tetrahydro-8-quinolinone; With ammonium acetate; 4 A molecular sieve; In dimethyl sulfoxide; at 85 ℃; for 0.0833333h;

5,6,7,8-tetrahydro-8-quinolinone; N,N-dimethyl-4'-(methoxy)benzylidene ammonium chloride; In dimethyl sulfoxide; at 120 ℃; for 16h; Further stages.;
DOI:10.1039/b316633c

Reference yield:

: 56826-69-8
5,6,7,8-tetrahydro-8-quinolinone

: N,N-dimethyl-4'-(methoxy)benzylidene ammonium chloride

: 6-(4'-methoxy)phenyl-7,8,13,14-tetrahydroquino<8,7-k><1,8>phenanthroline

: 148066-20-0
7-(4'-methoxy)phenyl-5,6,8,9-tetrahydroquino<8,7-b><1,10>phenanthroline

Guidance literature:: 5,6,7,8-tetrahydro-8-quinolinone; With ammonium acetate; In N,N-dimethyl-formamide;

N,N-dimethyl-4'-(methoxy)benzylidene ammonium chloride; In N,N-dimethyl-formamide; Further stages.;
DOI:10.1039/b316633c

Reference yield: 60.0%

: 108-89-4
picoline

: 14104-20-2
silver tetrafluoroborate

: 12266-72-7
1,5-cyclooctadienediiodoplatinum(II)

: 148066-20-0
7-(4'-methoxy)phenyl-5,6,8,9-tetrahydroquino<8,7-b><1,10>phenanthroline

: [Pt(5,6,8,9-tetrahydro-7-(4'-methoxyphenyl)quino[8,7-b][1,10]phenanthroline)(4-picoline)][BF₄]2

Guidance literature:: In acetone; acetonitrile; byproducts: AgI; AgBF4 was added to suspn. of Pt-complex in acetone, stirred at room temp., filtered, suspn. of ligand in MeCN was added, stirred at room temp. for 30 min, centrifuged, suspended in MeCN, treated with 4-picoline for 30 min under Ar; Et2O was added, recrystd. from MeCN by slow diffusion of Et2O vapour;
DOI:10.1039/b316633c