dodecahydrooxanthrene

Base Information

• Chemical Name: dodecahydrooxanthrene
• CAS No.: 25500-50-9
• Molecular Formula: C₁₂H₂₀O₂
• Molecular Weight: 196.29
• Mol file: 25500-50-9.mol

Synonyms:dodecahydrooxanthrene

Chemical Property of dodecahydrooxanthrene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of dodecahydrooxanthrene

There total 6 articles about dodecahydrooxanthrene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

1-(cyclohex-2-enyloxy)naphthalene → dodecahydrooxanthrene (25500-50-9) + 2-(cyclohex-2-enyl)naphthalen-1-ol (266338-24-3) + 4-(cyclohex-2-enyl)naphthalen-1-ol

Guidance literature:

With toluene-4-sulfonic acid; In diethyl ether; toluene; at 20 ℃; for 24h;

DOI:10.3390/molecules21040503

Reference yield:

phenol (108-95-2,27073-41-2) → dodecahydrooxanthrene (25500-50-9) + 4-(2-cyclohexen-1-yl)phenol (40141-05-7) + 3-(2-hydroxyphenyl)cyclohexene (14003-77-1)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate; sodium iodide / acetone / 12 h / Reflux

2: toluene-4-sulfonic acid / toluene; diethyl ether / 24 h / 20 °C

With potassium carbonate; toluene-4-sulfonic acid; sodium iodide; In diethyl ether; acetone; toluene;

DOI:10.3390/molecules21040503

Reference yield:

α-naphthol (90-15-3) + rac-3-bromocyclohexene (1521-51-3,113667-32-6) → dodecahydrooxanthrene (25500-50-9) + 4-(cyclohex-2-enyl)naphthalen-1-ol

Guidance literature:

Multi-step reaction with 2 steps

1: potassium carbonate; sodium iodide / acetone / 12 h / Reflux

2: toluene-4-sulfonic acid / toluene; diethyl ether / 24 h / 20 °C

With potassium carbonate; toluene-4-sulfonic acid; sodium iodide; In diethyl ether; acetone; toluene;

DOI:10.3390/molecules21040503

upstream raw materials:

dioxin

acetic acid

phenol

α-naphthol