{Fe₄O₂(bis(N-methylimidazol-2-yl)carbinol)2(bis(N-methylimidazol-2-yl)carbinolate)2(O₂CPh)4}Cl₂*5H₂O*2CH₃CN

Base Information

• Chemical Name: {Fe₄O₂(bis(N-methylimidazol-2-yl)carbinol)2(bis(N-methylimidazol-2-yl)carbinolate)2(O₂CPh)4}Cl₂*5H₂O*2CH₃CN
• CAS No.: 111410-35-6
• Molecular Formula: 2C₂H₃N*C₆₄H₆₆Fe₄N₁₆O₁₄*2Cl*5H₂O
• Molecular Weight: 1749.8
• Mol file: 111410-35-6.mol

Synonyms:{Fe₄O₂(bis(N-methylimidazol-2-yl)carbinol)2(bis(N-methylimidazol-2-yl)carbinolate)2(O₂CPh)4}Cl₂*5H₂O*2CH₃CN

Chemical Property of {Fe₄O₂(bis(N-methylimidazol-2-yl)carbinol)2(bis(N-methylimidazol-2-yl)carbinolate)2(O₂CPh)4}Cl₂*5H₂O*2CH₃CN

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of {Fe₄O₂(bis(N-methylimidazol-2-yl)carbinol)2(bis(N-methylimidazol-2-yl)carbinolate)2(O₂CPh)4}Cl₂*5H₂O*2CH₃CN

There total 1 articles about {Fe₄O₂(bis(N-methylimidazol-2-yl)carbinol)2(bis(N-methylimidazol-2-yl)carbinolate)2(O₂CPh)4}Cl₂*5H₂O*2CH₃CN which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

sodium benzoate (532-32-1) + bis(1-methyl-2-imidazolyl)hydroxymethane (67319-03-3) + (Et4N)2(Fe2OCl6) (87495-23-6) → {Fe4O2(bis(N-methylimidazol-2-yl)carbinol)2(bis(N-methylimidazol-2-yl)carbinolate)2(O2CPh)4}Cl2*5H2O*2CH3CN (111410-35-6) + tetraethylammonium chloride (56-34-8) + triethylamine hydrochloride (554-68-7) + sodium chloride (7647-14-5)

Guidance literature:

In dichloromethane; triethylamine; acetonitrile; mixt. of the Fe complex in CH3CN and Na benzoate stirred for 0.5 h; mixt. of BICOH in CH3CN/CH2Cl2 and Et3N stirred for 1 h and added to first mixt.; reaction mixt. stirred for 1 h; filtration, solvents removed in vac.; solid washed with hexane/CHCl3; resulting oil dried overnight under vac.; recrystn. from CH3CN; elem. anal.;

upstream raw materials:

sodium benzoate

bis(1-methyl-2-imidazolyl)hydroxymethane

(Et₄N)2(Fe₂OCl₆)