3-(1-methyl-1-azabicyclo<2.2.2>octyl) 2-hydroxy-3-(4-morpholinyl)-2-phenylpropionate iodide

Base Information

Chemical Name:3-(1-methyl-1-azabicyclo<2.2.2>octyl) 2-hydroxy-3-(4-morpholinyl)-2-phenylpropionate iodide
CAS No.:122846-70-2
Molecular Formula:C₂₁H₃₁N₂O₄*I
Molecular Weight:502.393
Hs Code.:

Synonyms:3-(1-methyl-1-azabicyclo<2.2.2>octyl) 2-hydroxy-3-(4-morpholinyl)-2-phenylpropionate iodide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(1-methyl-1-azabicyclo<2.2.2>octyl) 2-hydroxy-3-(4-morpholinyl)-2-phenylpropionate iodide

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Technology Process of 3-(1-methyl-1-azabicyclo<2.2.2>octyl) 2-hydroxy-3-(4-morpholinyl)-2-phenylpropionate iodide

There total 3 articles about 3-(1-methyl-1-azabicyclo<2.2.2>octyl) 2-hydroxy-3-(4-morpholinyl)-2-phenylpropionate iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 122846-65-5
1-Azabicyclo [2.2.2]octan-3-yl 2-Hydroxy-3-(4-morpholinyl)-2-phenylpropionate

: 74-88-4
methyl iodide

: 122846-70-2
3-(1-methyl-1-azabicyclo<2.2.2>octyl) 2-hydroxy-3-(4-morpholinyl)-2-phenylpropionate iodide

Guidance literature:: In diethyl ether; for 24h; Ambient temperature;
DOI:10.1021/jm00163a050

Reference yield:

: 19780-36-0
ethyl α-phenylglycidate

: 122846-70-2
3-(1-methyl-1-azabicyclo<2.2.2>octyl) 2-hydroxy-3-(4-morpholinyl)-2-phenylpropionate iodide

Guidance literature:: Multi-step reaction with 3 steps

1: 63.2 percent / ethanol / 18 h / Heating

2: 1.) Na / 1.) benzene, reflux, 1 h, 2.) reflux, 18 h

3: 86 percent / diethyl ether / 24 h / Ambient temperature

With sodium; In diethyl ether; ethanol;
DOI:10.1021/jm00163a050

Reference yield:

: 122846-56-4
ethyl 2-hydroxy-3-(4-morpholinyl)-2-phenylpropionate

: 122846-70-2
3-(1-methyl-1-azabicyclo<2.2.2>octyl) 2-hydroxy-3-(4-morpholinyl)-2-phenylpropionate iodide

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) Na / 1.) benzene, reflux, 1 h, 2.) reflux, 18 h

2: 86 percent / diethyl ether / 24 h / Ambient temperature

With sodium; In diethyl ether;
DOI:10.1021/jm00163a050