Aminomethyl-phosphonic acid benzyl ester 3-[benzyloxycarbonyl-(4-benzyloxycarbonylamino-butyl)-amino]-propyl ester

Base Information

Chemical Name:Aminomethyl-phosphonic acid benzyl ester 3-[benzyloxycarbonyl-(4-benzyloxycarbonylamino-butyl)-amino]-propyl ester
CAS No.:197971-41-8
Molecular Formula:C₃₁H₄₀N₃O₇P
Molecular Weight:597.648
Hs Code.:

Synonyms:Aminomethyl-phosphonic acid benzyl ester 3-[benzyloxycarbonyl-(4-benzyloxycarbonylamino-butyl)-amino]-propyl ester

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Chemical Property of Aminomethyl-phosphonic acid benzyl ester 3-[benzyloxycarbonyl-(4-benzyloxycarbonylamino-butyl)-amino]-propyl ester

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Technology Process of Aminomethyl-phosphonic acid benzyl ester 3-[benzyloxycarbonyl-(4-benzyloxycarbonylamino-butyl)-amino]-propyl ester

There total 8 articles about Aminomethyl-phosphonic acid benzyl ester 3-[benzyloxycarbonyl-(4-benzyloxycarbonylamino-butyl)-amino]-propyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 197971-40-7
(1,3-Dioxo-1,3-dihydro-isoindol-2-ylmethyl)-phosphonic acid benzyl ester 3-[benzyloxycarbonyl-(4-benzyloxycarbonylamino-butyl)-amino]-propyl ester

: 197971-41-8
Aminomethyl-phosphonic acid benzyl ester 3-[benzyloxycarbonyl-(4-benzyloxycarbonylamino-butyl)-amino]-propyl ester

Guidance literature:: With hydrazine hydrate; In methanol; for 24h; Ambient temperature;
DOI:10.1021/jm970414b

Reference yield:

: 197971-39-4
(1,3-Dioxo-1,3-dihydro-isoindol-2-ylmethyl)-phosphonic acid monobenzyl ester

: 197971-41-8
Aminomethyl-phosphonic acid benzyl ester 3-[benzyloxycarbonyl-(4-benzyloxycarbonylamino-butyl)-amino]-propyl ester

Guidance literature:: Multi-step reaction with 2 steps

2: 81 percent / H₂NNH₂

With hydrazine; 1: Esterification / 2: hydrazinolysis;
DOI:10.1080/10426509908546195

Reference yield:

: 197971-38-3
{4-[Benzyloxycarbonyl-(3-hydroxy-propyl)-amino]-butyl}-carbamic acid benzyl ester

: 197971-41-8
Aminomethyl-phosphonic acid benzyl ester 3-[benzyloxycarbonyl-(4-benzyloxycarbonylamino-butyl)-amino]-propyl ester

Guidance literature:: Multi-step reaction with 2 steps

2: 81 percent / H₂NNH₂

With hydrazine; 1: Esterification / 2: hydrazinolysis;
DOI:10.1080/10426509908546195