Hexadecanoic acid (S)-1-hexadecanoyloxymethyl-2-(hydroxy-phenoxy-phosphoryloxy)-ethyl ester

Base Information

• Chemical Name: Hexadecanoic acid (S)-1-hexadecanoyloxymethyl-2-(hydroxy-phenoxy-phosphoryloxy)-ethyl ester
• CAS No.: 124402-60-4
• Molecular Formula: C₄₁H₇₃O₈P
• Molecular Weight: 725

Synonyms:Hexadecanoic acid (S)-1-hexadecanoyloxymethyl-2-(hydroxy-phenoxy-phosphoryloxy)-ethyl ester

Chemical Property of Hexadecanoic acid (S)-1-hexadecanoyloxymethyl-2-(hydroxy-phenoxy-phosphoryloxy)-ethyl ester

Chemical Property:

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Technology Process of Hexadecanoic acid (S)-1-hexadecanoyloxymethyl-2-(hydroxy-phenoxy-phosphoryloxy)-ethyl ester

There total 4 articles about Hexadecanoic acid (S)-1-hexadecanoyloxymethyl-2-(hydroxy-phenoxy-phosphoryloxy)-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-O-benzyl-2,3-di-O-hexadecanoyl-sn-glycerol (90365-30-3) → Hexadecanoic acid (S)-1-hexadecanoyloxymethyl-2-(hydroxy-phenoxy-phosphoryloxy)-ethyl ester (124402-60-4)

Guidance literature:

Multi-step reaction with 2 steps

1: 90 percent / H₂ / 5percent Pd/C / ethanol / 2.5 h / 40 °C / 2585.7 Torr

2: pyridine / CH₂Cl₂ / 1.5 h

With pyridine; hydrogen; palladium on activated charcoal; In ethanol; dichloromethane;

DOI:10.1021/jm00164a027

Reference yield:

1,2-di-O-palmitoyl-sn-glycerol (6076-30-8) + O-phenyl phosphorodichloridate (770-12-7) → Hexadecanoic acid (S)-1-hexadecanoyloxymethyl-2-(hydroxy-phenoxy-phosphoryloxy)-ethyl ester (124402-60-4)

Guidance literature:

With pyridine; In dichloromethane; for 1.5h;

DOI:10.1021/jm00164a027

Reference yield:

1,2-dipalmitoyl-sn-glycerol (30334-71-5) + O-phenyl phosphorodichloridate (770-12-7) → Hexadecanoic acid (R)-1-hexadecanoyloxymethyl-2-(hydroxy-phenoxy-phosphoryloxy)-ethyl ester (124402-60-4)

Guidance literature:

With pyridine; In dichloromethane; for 1.5h;

DOI:10.1021/jm00164a027

upstream raw materials:

1,2-di-O-palmitoyl-sn-glycerol

O-phenyl phosphorodichloridate

1-O-benzyl-2,3-di-O-hexadecanoyl-sn-glycerol

1,2-dipalmitoyl-sn-glycerol

Downstream raw materials:

Hexadecanoic acid (R)-1-hexadecanoyloxymethyl-2-[((3aR,4S,4aR,7aS,8S,8aR)-8-hydroxy-2,2,6,6-tetramethyl-hexahydro-benzo[1,2-d;4,5-d']bis[1,3]dioxol-4-yloxy)-phenoxy-phosphoryloxy]-ethyl ester

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